Micro Small SPS Plasma Sintering Furnace Advanced Material Sintering System

Vacuum Hot Press Furnace

Micro Small SPS Plasma Sintering Furnace Advanced Material Sintering System

Item Number: TU-VH10

Maximum Temperature: 2300°C Heating Rate: ≤800°C/min Maximum Force: 3 tons
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Product Overview

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This spark plasma sintering furnace represents the forefront of rapid densification technology for advanced materials. By applying pulsed DC current directly through the powder compact within a conductive die, it generates internal resistive heating that activates sintering mechanisms instantaneously. This approach eliminates the slow heat transfer limitations of conventional radiation or convection furnaces, enabling heating rates as high as 800°C/min. The result is fully dense components with exceptional microstructural control achieved in remarkably short cycle times—often just a few minutes. Its compact, benchtop-friendly design makes it an excellent fit for modern research laboratories where space and efficiency are critical.

Designed to serve a wide spectrum of materials research, this furnace excels in processing refractory metals (tungsten, molybdenum, niobium), engineering ceramics (alumina, silicon carbide, boron carbide), cermets (WC-Co, TiC-Ni), and functional gradient materials. Typical applications include the development of new alloy compositions, production of small-scale ceramic prototypes, and rapid screening of novel composite formulations. Researchers in metallurgy, ceramics, nanotechnology, and energy materials value its ability to sinter powders into high-density bodies while minimizing grain growth—a challenge that plagues conventional sintering methods. The system’s versatility extends to emerging fields such as high-entropy alloys and thermoelectric materials.

Built for sustained performance in rigorous laboratory settings, the furnace incorporates a robust horizontal chamber with a side-opening door that permits easy loading and unloading of samples. Precision vacuum control achieves ultimate levels of 6.7×10⁻⁴ Pa, and the servo-electric press delivers up to 3 tons of force with fluctuations below ±150 N—critical for maintaining consistent density across runs. The integrated PLC with a touchscreen interface not only automates complex temperature-pressure-vacuum profiles but also provides comprehensive data logging with real-time curve visualization, historical archiving, and user-level access controls. These features, combined with a sturdy construction and proven component reliability, make this unit a trusted tool in academic and industrial R&D labs worldwide.

Key Features

  • Rapid Joule Heating Technology: Pulsed DC current passes directly through the conductive die or sample, generating heat internally at the particle contacts. This eliminates thermal lag, resulting in heating rates up to 800°C/min and total sintering cycles as short as 2–5 minutes for many materials.
  • High-Temperature Capability: The furnace achieves a maximum operating temperature of 2300°C, enabling the sintering of ultra-high-temperature ceramics (UHTCs), refractory metals, and composites that require extreme thermal conditions for densification.
  • Ultra-Clean Vacuum Atmosphere: A cold-state ultimate vacuum of 6.7×10⁻⁴ Pa and a low pressure rise rate of just 2 Pa/h provide a pristine environment for processing reactive and high-purity materials, avoiding unwanted oxidation or contamination.
  • Servo-Electric Precision Press: The press delivers up to 3 tons of axial force with closed-loop servo control. Pressure stability is maintained within ±150 N, and displacement accuracy is better than 0.01 mm, enabling precise densification and final part dimension control.
  • Intelligent Process Automation: The touchscreen PLC controller allows programming of multistep profiles for temperature, pressure, and vacuum. All process data are recorded in real time and can be downloaded via USB for analysis, while recipe storage and user permissions enhance reproducibility and security.
  • Ergonomic and Compact Design: The horizontal side-opening structure provides unobstructed access for sample handling while maintaining a small footprint. This design simplifies loading of dies and tooling, speeding up experimental turnaround.
  • Dual Pressure Control Modes: Users can choose between force control and position control, adapting the press operation to the specific needs of the material—whether maintaining constant pressure or achieving a targeted displacement.
  • Versatile Sample Geometry: With a press head diameter of 50 mm and a stroke of 0–60 mm, the system accommodates sample diameters from 8 to 15 mm and a variety of die heights, making it adaptable to many experimental setups.
  • Exceptional Energy Efficiency: Direct resistive heating significantly reduces energy consumption compared to conventional furnaces, translating into lower operating costs and a smaller carbon footprint for the laboratory.
  • Robust Safety Systems: Integrated interlocks, over-temperature alarms, and vacuum monitoring ensure safe operation even at maximum parameters, protecting both the operator and the equipment from potential mishaps.

Applications

Application Description Key Benefit
Refractory Metal Components Sintering of dense tungsten, molybdenum, niobium, and tantalum parts for high-temperature structural applications such as heating elements, x-ray targets, and crucibles. Achieves high density above 95% theoretical while keeping grain size small, ensuring good mechanical strength and oxidation resistance.
Transparent Polycrystalline Ceramics Processing of pure and doped Al₂O₃, MgAl₂O₄ spinel, and YAG for optical windows, laser hosts, and transparent armor. Short sintering time prevents grain coarsening, yielding high in-line transmission and optical clarity without sintering aids.
Ultra-High-Temperature Ceramics (UHTCs) Consolidation of bordies (ZrB₂, HfB₂) and carbides (TaC, HfC) for hypersonic nose tips, rocket nozzles, and thermal protection systems. Produces fully dense, oxidation-resistant components with superior mechanical properties at extreme temperatures.
Nanostructured Bulk Materials Sintering of nano-powders (metals, oxides, carbides) while limiting grain growth to preserve nanocrystallinity for enhanced properties. Retains nano-scale features, leading to exceptional hardness, wear resistance, and unique functional behaviors.
Hardmetal Cutting Tools Fabrication of WC-Co, TiC-Ni, and other cermets for precision cutting inserts, mining tools, and wear-resistant parts. Uniform binder distribution and controlled carbide grain size yield an optimal balance of toughness and hardness under heavy loads.
Thermoelectric Generators Consolidation of Bi₂Te₃, skutterudites, and half-Heusler compounds for solid-state energy conversion and cooling devices. Preserves fine microstructure and stoichiometry, crucial for achieving high thermoelectric figure of merit (ZT).
Functionally Graded Materials Creating spatial gradients in composition, porosity, or particle size for thermal barrier coatings, biomedical implants, and graded joints. Enables precise control of property transitions without delamination, using custom layering schedules.
Intermetallic Alloys for Aerospace Processing of TiAl, NiAl, and MoSi₂ for lightweight turbine blades, structural panels, and high-temperature engine components. Produces crack-free, isotropic near-net-shape parts with excellent strength retention at elevated temperatures.

Technical Specifications

The table below details the technical specifications for the TU-VH10 compact spark plasma sintering furnace.

Parameter Value
Power Supply Three-phase 380 V, 50 Hz
Rated Power Single-phase 380 V, 30 kW ±10%
Operating Voltage / Current DC 1–10 V, DC 0–3000 A
Maximum Temperature 2300°C
Structure Horizontal side-opening
Sample Size Diameter 8–15 mm
Heating Rate ≤800°C/min
Ultimate Vacuum (cold) ≤6.7×10⁻⁴ Pa
Pressure Rise Rate 2 Pa/h
Maximum Force 3 tons (digital display, automatic regulation & hold, servo-electric)
Press Head Diameter Ф50 mm
Pressure Fluctuation ≤±150 N
Displacement Accuracy ≥0.01 mm
Pressure Stroke 0–60 mm (digital display)
Pressure Control Servo-electric
Control System Touchscreen + PLC; real-time data recording, storage, download for temperature, vacuum, pressure, displacement; curve visualization; recipe programming; user permission management

Why Choose This Product

  • Dramatically Reduced Time-to-Result: With heating rates of up to 800°C/min and short sintering cycles, this furnace condenses processes that typically take hours into mere minutes, accelerating your research timeline and enabling rapid experimentation.
  • Precision and Repeatability You Can Trust: Closed-loop servo pressure control, high-accuracy displacement feedback, and stable vacuum performance ensure that every run delivers consistent, reliable data—essential for high-stakes research and quality-critical small-batch production.
  • Engineered for Long-Term Dependability: From the water-cooled power electrodes to the reinforced vacuum chamber, every component is selected and integrated for durability under continuous use, minimizing downtime and maintenance expenses.
  • Customizable to Your Research Needs: Our engineering team offers tailored solutions including specialized tooling, controlled atmosphere options (argon, nitrogen, forming gas), and software customizations to address unique experimental requirements.
  • Comprehensive Service and Support: Our global network of experienced application engineers and service technicians provides installation, training, and ongoing technical support to ensure your system operates at peak performance for years to come.

Contact our sales team today to discuss your specific requirements and receive a personalized quote. Let us help you unlock new possibilities in materials development with a solution engineered for your success.

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