1000C Mini Tube Furnace with 20mm Quartz Tube and Vacuum Flanges for Material Science Research and Controlled Atmosphere Small Sample Processing

Tube Furnace

1000C Mini Tube Furnace with 20mm Quartz Tube and Vacuum Flanges for Material Science Research and Controlled Atmosphere Small Sample Processing

Item Number: TU-14

Maximum Temperature: 1000°C Processing Tube Size: 20 mm OD x 192 mm Length Programmable Segments: 30 Segments PID Control
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Product Overview

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This high-performance mini thermal processing system is engineered to meet the rigorous demands of modern material science and industrial R&D laboratories. Designed as a compact yet powerful solution for high-temperature applications, the equipment provides a stable and controlled environment for heating small samples up to 1000°C. Its primary value proposition lies in its extreme versatility, allowing researchers to conduct experiments under vacuum or specific gas atmospheres with high precision. By combining a small footprint with industrial-grade heating capabilities, this unit serves as an essential tool for pioneering research where space is at a premium but performance cannot be compromised.

The system is particularly well-suited for diverse applications including chemical vapor deposition (CVD), vapor-liquid-solid (VLS) nanowire growth, and sophisticated gas analysis. Because the furnace and its controller are designed as separable modules, the equipment offers unparalleled flexibility in laboratory setup. This allows the unit to be integrated into complex experimental rigs or placed within specialized environments such as gloveboxes. Whether used for semiconductor research, battery material testing, or metallurgical analysis, the unit provides the consistent thermal profiles required for reproducible scientific results.

Reliability is the cornerstone of this thermal processing system. Built with high-quality components, including a durable Fe-Cr-Al alloy heating element doped with molybdenum and a high-purity fused quartz tube, the equipment is designed for longevity and continuous operation in demanding environments. The inclusion of stainless steel vacuum flanges and advanced safety shielding ensures that the system operates safely even at its peak temperature of 1000°C. For procurement teams and lab managers, this furnace represents a robust investment in high-accuracy thermal equipment that will deliver consistent performance throughout its long operational life.

Key Features

  • Precision PID Temperature Regulation: The integrated temperature controller utilizes advanced Proportional-Integral-Derivative (PID) logic and auto-tune functions to maintain an accuracy of ±1°C, ensuring that even the most sensitive material transformations occur under exact thermal conditions.
  • Sophisticated 30-Segment Programming: To accommodate complex thermal cycles, the system allows for the programming of up to 30 distinct segments for heating, dwelling, and cooling rates, providing researchers with total control over the processing timeline.
  • Modular and Separable Architecture: The furnace unit is physically separable from the control console, a design feature that allows the heating chamber to be placed inside a glovebox while the electronics remain external, protecting the controller from harsh environments and facilitating easier maintenance.
  • Dual-Orientation Mounting Versatility: Engineered with a flexible frame, this equipment can be operated in either a horizontal or vertical position, making it adaptable to various experimental setups such as gravity-fed deposition or standard horizontal annealing.
  • High-Integrity Vacuum Sealing: Equipped with stainless steel flanges, including a KF25 quick clamp and a screw-tightened end with a 1/4" gas inlet, the system can achieve a vacuum pressure of 20 mTorr, essential for high-purity processing and oxygen-sensitive material synthesis.
  • Enhanced Safety Protection: A specialized protective shield is mounted over the furnace body to prevent accidental contact with the high-temperature surface during operation at 800°C and above, prioritizing operator safety in a busy laboratory setting.
  • Optimized Heating Zone Efficiency: The 55mm heating zone is designed to provide a 20mm constant temperature region (±5°C), allowing for uniform thermal distribution across small samples and reducing the risk of thermal gradients that could affect experimental integrity.
  • Durable Material Construction: The use of Mo-doped Fe-Cr-Al alloy heating elements ensures excellent resistance to oxidation and thermal cycling fatigue, while the high-purity quartz tube maintains chemical inertness during gas-phase reactions.
  • Glovebox Compatibility: The compact dimensions of the heating unit are specifically calculated to allow it to pass through standard glovebox airlocks, enabling specialized processing in inert or moisture-free atmospheres.
  • Built-in Diagnostic Protection: The controller features integrated protection against overheated states and broken thermocouples, automatically shutting down power to prevent damage to the equipment or the processing tube in the event of a sensor failure.

Applications

Application Description Key Benefit
Nanowire Synthesis (VLS) Growing crystalline structures using the Vapor-Liquid-Solid method in a controlled 1000°C environment. High temperature stability ensures uniform wire diameter and crystal quality.
Small Sample Annealing Relieving internal stresses in specialized metal alloys or ceramic pellets under vacuum. Precision cooling segments prevent thermal shock and material cracking.
Chemical Vapor Deposition Depositing thin films onto substrates by introducing reactive gases into the quartz tube. Excellent vacuum integrity prevents contamination from ambient air.
Gas Analysis Heating samples to observe off-gassing or catalytic reactions with integrated gas inlet/outlet. Precise control over gas flow and temperature allows for accurate kinetic data.
Glovebox Research Processing oxygen-sensitive battery materials inside an inert atmosphere glovebox. Modular design allows the heating unit to fit through airlocks while the controller stays outside.
Semiconductor Doping Introducing dopants into small wafers or substrates at controlled high temperatures. Uniform thermal zone ensures consistent dopant penetration across the sample surface.
Catalyst Testing Evaluating the efficiency of new catalyst materials under specific thermal and atmospheric conditions. 30-segment programming allows for rapid screening of multiple temperature steps.

Technical Specifications

General Performance and Electrical

Parameter Value (Model: TU-14)
Maximum Temperature 1000 °C (< 1 hour duration)
Continuous Working Temperature 900 °C
Maximum Heating Rate 10 °C per minute
Temperature Accuracy ± 1 °C
Power Output 500W Maximum
Voltage Compatibility Selectable 110V or 220V AC (50/60 Hz)
Heating Zone Length 2.16" (55 mm)
Constant Temperature Zone 0.8" (20 mm) at ± 5 °C

Material and Hardware Components

Component Specification for TU-14
Processing Tube Fused Quartz Tube: 20 mm OD x 17 mm ID x 192 mm Length
Heating Elements Fe-Cr-Al Alloy doped by Mo
Thermocouple K type high-sensitivity sensor
Vacuum Flange A KF25 quick clamp flange (without valve)
Vacuum Flange B Screw-tighten flange with 1/4" gas inlet
Heat Radiation Shielding Two ceramic tube blocks included as standard
Scald Protection External mounted protective shield for 800°C+ safety

Operational and Compliance Data

Feature Detail
Vacuum Capability 20 mTorr achievable with mechanical pump
Control System 30-segment programmable PID with auto-tune
Mounting Positions Horizontal or Vertical orientation
Separability Furnace unit is detachable from the control unit
Shipping Weight 50 lbs
Compliance CE Certified (NRTL/UL61010/CSA optional)
Warranty One-year limited warranty with lifetime support

Why Choose This Furnace

  • Unmatched Versatility for Small-Scale R&D: The separable design of this unit makes it the premier choice for laboratories needing to integrate heating systems into gloveboxes or custom vacuum systems, providing flexibility that standard integrated furnaces cannot match.
  • Precision-Engineered Thermal Accuracy: Our PID control systems are calibrated to provide exceptional stability, ensuring that your research results are dictated by your experimental variables rather than thermal fluctuations.
  • Industrial-Grade Durability in a Compact Form: By utilizing Mo-doped heating elements and high-purity quartz, this system offers the same robust longevity as our larger industrial models, making it a sustainable investment for long-term research programs.
  • Global Safety and Compliance Standards: Every unit is CE certified, with options for UL and CSA certification, ensuring that the equipment meets the stringent safety requirements of academic and corporate institutions worldwide.
  • Expert Support and Customization: Beyond the hardware, we provide comprehensive lifetime technical support and can offer customization in tubes and flanges to meet specific process requirements.

Please contact our technical sales team today to request a quote or to discuss how this specialized mini furnace can be integrated into your next research project.

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