Tube Furnace
High Temperature Horizontal Electrical Assisted Sintering Furnace with 3KW Programmable Power Source for Advanced Ceramic Materials
Item Number: TU-86
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Product Overview


This high-temperature horizontal thermal processing system represents a significant advancement in material science instrumentation, specifically engineered for electric-assisted sintering (EAS) and flash sintering protocols. By combining a precision-controlled 1600°C horizontal tube furnace with an integrated 3KW programmable AC power source, the equipment allows researchers to investigate the transformative effects of electric fields on ceramic densification. This integrated approach enables the simultaneous application of thermal energy and controlled electrical currents, facilitating the sintering of materials at significantly lower temperatures and shorter durations than traditional methods.
The system is primarily utilized in cutting-edge laboratory environments and industrial R&D centers focusing on technical ceramics, solid-state battery electrolytes, and high-performance composites. Its horizontal configuration is optimized for specialized sample loading, featuring a slidable flange system that streamlines the placement of delicate ceramic specimens within the high-heat zone. Beyond flash sintering, the unit serves as a versatile platform for atmosphere-controlled heat treatments, chemical vapor deposition (CVD), and powder calcination, making it an indispensable asset for institutions pushing the boundaries of solid-state ionics and structural ceramic engineering.
Engineered for high-duty cycle performance under demanding laboratory conditions, this system emphasizes reliability and precision. Every component, from the high-purity alumina process tube to the platinum electrode feedthroughs, is selected to withstand extreme thermal gradients and electrical loads. This robust construction ensures that users can achieve repeatable, high-density results in every cycle, providing the confidence necessary for peer-reviewed research and the development of commercial-grade advanced materials. The equipment is built to maintain rigorous vacuum integrity and temperature uniformity, meeting the exacting standards of the international material science community.
Key Features
- Integrated 3KW Programmable AC Source: The system includes a dedicated power supply capable of delivering up to 208 VAC with 3000W capacity, allowing for the precise application of electric fields to trigger flash sintering and explore electrical-assisted material transformations.
- Precision Multi-Step Temperature Control: An advanced PID controller manages the thermal cycle through 30 programmable segments with ±1°C accuracy, ensuring the heating rates and soak times meet the strict requirements of complex material synthesis.
- High-Purity Alumina Processing Tube: Equipped with a standard 80mm OD alumina tube, the furnace provides a chemically inert and thermally stable environment suitable for continuous operation at 1600°C, preventing contamination in sensitive ceramic samples.
- Slidable Vacuum Flange and Sample Fixture: The engineering of the right-side flange allows it to slide easily along the support rails, facilitating effortless sample loading and unloading while protecting the internal heating elements and sample alignment.
- Platinum Electrode Feedthroughs: High-conductivity Ø1 mm platinum wires are utilized for the electrical feedthroughs, ensuring stable current delivery up to 15A within the high-temperature zone without oxidation or material degradation.
- Dual-Zone Thermal Management: The furnace features an 18-inch heating zone with a 6-inch constant temperature region maintained within ±3°C, providing the thermal uniformity required for consistent densification across the entire sample length.
- Quartz Observation Window: A 30mm diameter quartz window integrated into the vacuum flange allows real-time visual monitoring of the sample during the flash sintering process, enabling researchers to observe plasma formation or material glowing effects.
- Advanced Safety and Protection: Built-in over-temperature and thermocouple failure protection systems automatically cut power to prevent equipment damage, while the programmable AC source includes overload and short-circuit protection for operator safety.
- Vacuum-Ready Sealing System: Stainless steel flanges with needle valves and mechanical gauges enable the system to reach vacuum levels of 10^-2 torr via mechanical pump, essential for processing materials sensitive to atmospheric oxidation.
- Customizable Control Options: While standard with a robust PID interface, the system can be upgraded to high-precision Eurotherm controllers with RS485 communication for automated data logging and remote process management via computer.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Flash Sintering Research | Investigating rapid densification of ceramic powders under high-strength AC electric fields. | Reduces sintering time from hours to seconds while lowering peak temperatures. |
| Solid-State Battery Development | Processing of solid electrolyte ceramics like LLZO or NASICON that require precise thermal and electrical control. | Achieves high ionic conductivity and grain boundary optimization. |
| Superconducting Material Synthesis | High-temperature annealing and sintering of ceramic superconductors in controlled atmospheres. | Enhances phase purity and critical current density through uniform thermal processing. |
| CVD / PECVD Processes | Growing thin films or carbon nanotubes using the furnace as a reactor with optional gas delivery systems. | Versatile platform for both thermal and plasma-enhanced deposition techniques. |
| High-Temperature Metallizing | Bonding ceramic components to metal substrates for aerospace or electronics applications. | Provides the precise atmosphere and temperature needed for robust hermetic seals. |
| Dielectric Property Analysis | Measuring the change in material properties at elevated temperatures under electrical load. | Integrated platinum wires allow for in-situ electrical measurements during heating. |
| Advanced Refractory Testing | Evaluating the thermal shock resistance and electrical resistivity of high-performance refractories. | High-temperature capability (1700°C max) allows for extreme environment simulation. |
Technical Specifications
| Specification Category | Parameter Details (TU-86) | Value / Description |
|---|---|---|
| Furnace Power | Input Voltage | 208-240 VAC, 50/60 Hz |
| Power Consumption | 5.2 KVA | |
| AC Power Source | Input Voltage | AC220V ±10%, 50/60Hz, Single Phase |
| Max Power Capacity | 3000 W | |
| Output Voltage Range | 20V - 208 VAC Adjustable | |
| Voltage Stability | ≤ 1% | |
| Protection | Overload, Over-temperature, Short-circuit | |
| Thermal Performance | Max Operating Temp | 1700°C |
| Continuous Operating Temp | 1600°C | |
| Heating Zone Length | 18" (457 mm) | |
| Constant Temp Zone | 6" (150 mm) within ±3°C | |
| Process Tube | Material | High-purity Alumina |
| Dimensions | Ø 2 3/8" x 40" (60mm OD x 54mm ID x 1000mm L) | |
| Control System | Controller Type | PID Automatic Control via SSR |
| Programming | 30 steps programmable | |
| Accuracy | ±1°C | |
| Thermocouple | B-type | |
| Vacuum & Sealing | Flange Material | Stainless Steel |
| Vacuum Limit | 10^-2 torr (Mechanical Pump) | |
| Observation Window | 30 mm dia. Quartz | |
| Sample Fixture | Built-in slidable flange with platinum leads | |
| Compliance | Standards | CE Certified (NRTL/UL61010 available upon request) |
Why Choose Us
- Engineered for Scientific Discovery: This system is not just a furnace; it is a specialized instrument designed to facilitate the emerging field of flash sintering, providing researchers with the integrated tools necessary for high-impact results.
- Industrial-Grade Thermal Stability: Built with premium B-type thermocouples and high-purity ceramic components, the unit maintains exceptional stability at temperatures up to 1600°C, ensuring the longevity of your investment.
- Precision Electrical Integration: The 3KW programmable AC source is specifically tuned to work in tandem with the furnace's thermal cycle, providing a seamless interface for applying electric fields with sub-1% stability.
- Versatile and Scalable Design: With options for multi-channel gas delivery systems and high-vacuum digital gauges, the equipment can be adapted from a basic sintering furnace to a sophisticated CVD or atmosphere-controlled reactor.
- Uncompromising Safety and Quality: CE certified and built with comprehensive protection circuits, this equipment provides a safe operating environment for university labs and industrial facilities alike.
Our technical team is ready to assist you in configuring this advanced sintering system for your specific research needs. Contact us today for a technical consultation or a formal quote to enhance your laboratory's capabilities.
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