High Temperature Oxygen and Inert Atmosphere Controlled Furnace 8 Liter 1700C Sintering System for Advanced Materials RD

Atmosphere Furnace

High Temperature Oxygen and Inert Atmosphere Controlled Furnace 8 Liter 1700C Sintering System for Advanced Materials RD

Item Number: TU-QF09

Maximum Temperature: 1700°C Chamber Capacity: 8 Liters (200x200x200mm) Atmosphere Compatibility: Air, 100% Oxygen, Inert Gases (Ar, N2)
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Product Overview

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This high-temperature thermal processing system represents a pinnacle of engineering for laboratories requiring precise atmosphere control and extreme thermal performance. Specifically designed for the sintering of materials under air, 100% oxygen, or inert atmospheres, this equipment provides the necessary environment for preparing high-purity oxide ceramics. The system's architecture is optimized for stability, utilizing high-quality alumina fiber bricks and high-performance heating elements to achieve temperatures up to 1700°C with exceptional uniformity and repeatability.

The primary use cases for this system span across advanced material science, with a particular focus on the preparation of high-nickel battery cathode materials which require strictly controlled oxygen levels. In addition to battery research, the unit is an essential tool for aerospace engineering, semiconductor development, and solid-state chemistry. Target industries include industrial R&D centers, university research labs, and specialized manufacturing facilities that demand uncompromising reliability in their thermal treatment processes.

Built for demanding industrial and laboratory conditions, the equipment ensures maximum performance through a robust double-layer steel structure. This design not only facilitates vacuum integrity but also provides a safe, cool-to-the-touch exterior shell during high-temperature operations. With integrated cooling mechanisms and precision-controlled gas flow systems, researchers can conduct experiments with total confidence in the unit's ability to maintain consistent thermal and atmospheric profiles over long durations.

Key Features

  • Precision Atmosphere Versatility: This system is engineered to handle various atmospheric conditions, including air, pure oxygen, and inert gases like Nitrogen and Argon. This flexibility allows researchers to tailor the environment to the specific stoichiometric needs of their materials, particularly for oxide ceramics.
  • High-Performance Molybdenum Disilicide Heating: Equipped with six sets of replaceable MoSi2 heating elements, the unit can reach operating temperatures between 600°C and 1700°C. These elements are designed for longevity and consistent heat output even in highly oxidizing environments.
  • Advanced Dual-Layer Steel Construction: The furnace features a heavy-duty double-layer steel casing with air-cooling fans and a water-cooled front door. This dual-cooling approach ensures structural integrity at maximum temperatures while protecting internal components and laboratory personnel.
  • Sophisticated Thermal Regulation: Utilizing a Eurotherm 3000 controller with 0.1°C resolution and 24 programmable segments, the system offers precise PID control. This ensures a stable temperature profile with an accuracy of ±2°C, minimizing thermal drift during critical sintering cycles.
  • Integrated PC Control and Data Acquisition: A built-in industrial computer manages both temperature and pressure parameters. The system automatically records temperature and pressure profiles directly to the hard disk, facilitating comprehensive data analysis and traceability for quality control.
  • Enhanced Safety and Alarm Systems: To protect both the equipment and the operator, the unit includes multi-point safety alerts. These include over-temperature protection, high/low-pressure alarms, and low water flow alerts, each managed by independent secondary controllers.
  • Superior Thermal Insulation: The chamber is lined with energy-saving 1800-grade fibrous alumina insulation and a high-purity Al2O3 coating. This provides excellent thermal reflectance and energy efficiency, reducing power consumption while protecting the heating elements.
  • Automated Pressure Management: The system features a pressure sensor and controller that maintain constant pressure during the heating cycle. With both manual and automatic purging modes, the unit allows for precise control of the internal environment between -0.06 to 0.03Mpa.
  • Complete Gas and Vacuum Integration: The front panel is equipped with two large float meters for gas flow control and a vacuum pump is included to enhance the purging process. This ensures the chamber is thoroughly cleared of residual air before introducing process gases.

Applications

Application Description Key Benefit
Battery Cathode Research Sintering high-nickel cathode materials (NMC/NCA) in controlled 100% oxygen environments. Ensures precise stoichiometry and electrochemical performance.
Oxide Ceramic Fabrication High-purity preparation of structural and functional ceramics like Alumina and Zirconia. Minimizes contamination and enhances material density.
Aerospace Component Testing Thermal stress testing of ceramic matrix composites under inert or oxidizing conditions. Simulates extreme operational environments with high repeatability.
Solid State Chemistry Synthesis of complex metal oxides and high-temperature superconductors. Provides the high thermal energy and atmosphere purity required for synthesis.
Metallurgy Specialized heat treatment of precious metals and alloys requiring argon shielding. Prevents oxidation and maintains material integrity during processing.
Semiconductor Processing Thermal annealing of wafers and ceramic substrates in inert atmospheres. Consistent thermal profiles prevent structural defects and warping.

Technical Specifications

Parameter Category Specification Details for Model TU-QF09
Model Identifier TU-QF09 Atmosphere-Controlled Box Furnace
Maximum Temperature 1700°C (duration < 60 minutes)
Working Temperature Range 800°C - 1600°C (Air/O2); 1000°C - 1600°C (Inert Gas)
Heating Chamber Dimensions 200mm x 200mm x 200mm (8" x 8" x 8")
Total Chamber Volume 8 Liters
Heating Elements 6 Sets of replaceable MoSi2 elements with Ni-coated copper connections
Insulation Material 1800 Grade energy-saving fibrous alumina with high purity Al2O3 coating
Temperature Control Eurotherm 3000 controller; 0.1°C resolution; 24-segment programmable
Temperature Accuracy ± 2.0°C
Heating Rate 5°C per minute
Thermocouple Type Dual B-type thermocouples (Control and Monitor/Alarm)
Pressure Control Range -0.06 Mpa to 0.03 Mpa with automatic pressure sensor
Vacuum Performance Low vacuum level 10-1 torr (at low temp); ~500 torr at high temperature
Power Supply AC 208 - 240V, Single Phase, 50/60 Hz
Maximum Current/Power 50 Amps / 7.5 kW
Gas Management Two integrated flow meters; Built-in pressure gauge and vacuum valves
Cooling Requirements 58L/min recirculating water cooling for door and casing
Data Logging Built-in PC for recording temp/pressure; WIFI remote operation optional
Max. Sample Load 100 kg
Regulatory Compliance CE Certified; NRTL/CSA available upon request

Why Choose This System

  • Engineered for Purity: The combination of high-purity alumina insulation and atmosphere-tight sealing makes this unit the industry standard for researchers working with oxygen-sensitive or high-purity oxide materials.
  • Proven Reliability: With its double-layer steel construction and water-cooled door design, the system is built to withstand the rigors of continuous high-temperature operation in industrial and academic R&D settings.
  • Precision and Protection: Dual-redundant safety features, including separate thermocouples for control and monitoring, provide an extra layer of protection for expensive samples and internal furnace components.
  • Versatile Integrated Controls: The built-in PC and Eurotherm controller offer a sophisticated interface for both manual and automated thermal cycles, ensuring data-driven results that are easily exportable for research documentation.
  • Scalable Thermal Solutions: As part of a comprehensive range of thermal equipment, this unit represents a premium investment in a platform known for durability, operational consistency, and long-term serviceability.

For customized configurations or a detailed quotation tailored to your specific material science requirements, please contact our technical sales team today.

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