High Magnetic Field Tube Furnace with Triple Layer Vacuum Jacket and Non Magnetic SS316L Construction for Material Annealing

Tube Furnace

High Magnetic Field Tube Furnace with Triple Layer Vacuum Jacket and Non Magnetic SS316L Construction for Material Annealing

Item Number: TU-C26

Maximum Temperature: 300 °C Construction Material: Non-Magnetic SS316L Heating Zone Length: 1000 mm
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Product Overview

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This high-precision thermal processing system is specifically engineered for material annealing applications within high-intensity magnetic environments. Utilizing specialized construction materials that exhibit nearly zero magnetic permeability, the equipment ensures that thermal treatments can be conducted inside superconducting high-field magnets without distorting magnetic flux or experiencing mechanical stress from magnetic attraction. This unit represents a critical tool for researchers focused on quantum materials, superconductivity, and advanced magnetism.

The system features a sophisticated triple-layer architectural design, integrating a heating element core, a dedicated sample chamber, and a vacuum/gas-insulated cooling jacket. This configuration allows for high-temperature operations while ensuring the external surface of the furnace remains at safe levels, preventing thermal interference with the surrounding superconducting magnet components. It is an essential solution for laboratory and industrial R&D facilities that require precise thermal control under extreme electromagnetic conditions.

Built for long-term reliability and consistency, the unit employs high-grade SS316L stainless steel for its structural components and advanced silicon carbide (SiC) heating elements. These choices reflect a commitment to durability and performance under demanding vacuum and high-temperature cycles. Procurement teams can trust this equipment to deliver repeatable results in sensitive experimental setups where standard tube furnaces would fail due to magnetic interference or thermal leakage.

Key Features

  • Non-Magnetic SS316L Construction: The entire furnace body is fabricated from high-grade SS316L stainless steel, chosen for its negligible magnetic permeability. This allows the equipment to be placed directly into high-field magnets without causing field distortion or experiencing force displacement.
  • Triple-Layer Thermal Management: The system utilizes a unique three-layer tube structure. An internal SiC filament provides the heat source, a secondary quartz layer houses the sample, and an outer gas-cooled jacket maintains the exterior wall temperature below 30ºC to protect external sensors and superconducting magnets.
  • High-Efficiency Silicon Carbide Heating: Center-spiral SiC filaments provide rapid and uniform heating within the core zone. This heating technology is chosen for its stability at elevated temperatures and its ability to operate effectively within vacuum-jacketed environments.
  • Precision PID Temperature Control: An advanced automatic PID controller features 30 programmable segments, allowing for complex ramp and soak profiles. The auto-tune function and ±1ºC accuracy ensure that delicate material transformations occur under strictly controlled conditions.
  • Integrated Safety Protection: The unit includes built-in safeguards against thermocouple failure and overheating. These features are critical for long-duration annealing processes where equipment integrity and sample safety are paramount.
  • Superior Vacuum Integrity: Designed to interface with high-vacuum systems, the equipment can achieve levels as low as 10^-5 Torr when paired with a molecular pump. The vacuum-sealed flanges ensure a contaminate-free environment for sensitive material processing.
  • Active Cooling Jacket: The specialized 90mm O.D. outer layer functions as a gas-cooled thermal barrier. This design prevents heat from radiating into the magnet bore, which is essential for maintaining the cryogenic stability of superconducting systems.
  • Flexible Gas Handling: Equipped standard with barbed hose fittings, the system can be upgraded with KF25 adapters or Swagelok fittings to accommodate high-purity gas delivery or higher throughput vacuum requirements.

Applications

Application Description Key Benefit
Superconducting Magnet Research Annealing samples directly inside a high-field magnet bore for in-situ property studies. Zero magnetic interference with the superconducting field.
Quantum Material Synthesis Thermal treatment of materials exhibiting quantum Hall effects or topological insulator properties. Precise temperature ramp control for crystal growth and phase shifts.
Magnetic Semiconductor Doping Processing of dilute magnetic semiconductors under controlled atmospheres and high fields. High vacuum integrity prevents sample oxidation or contamination.
NMR Sample Preparation Homogenizing samples for high-resolution Nuclear Magnetic Resonance spectroscopy. Uniform heating zone ensures sample consistency across the entire volume.
Cryogenic Component Testing Stress-relieving thermal cycles for components intended for use in ultra-low temperature environments. Low external wall temperature protects surrounding cryogenic hardware.
Thin Film Annealing Post-deposition heat treatment of thin films under vacuum or inert gas. Minimal thermal shock to the quartz tube due to controlled flow rates.

Technical Specifications

Parameter Specifications for TU-C26
Model Identifier TU-C26
Furnace Structure Triple-layer construction: Heating element layer, SiC sheath layer, Sample layer, and Outer gas-cooled jacket
Core Heating Element Center spiral type SiC filament (25mm OD x 20mm ID x 400mm L)
Intermediate Sheath Quartz tube (30mm ID x 36mm OD x 622mm L)
Sample Layer 36mm ID x 58mm OD x 622mm L with vacuum sealed flange
Cooling Layer 58mm ID x 90mm OD x 622mm L (designed to keep exterior wall < 30ºC)
Power Supply 208 - 240 VAC, single phase, 2000W
Maximum Temperature 300 °C (for durations < 1 hour)
Continuous Working Temp 250 °C
Max. Heating Rate 10 °C / minute
Heating Zone Length 1000 mm
Constant Temperature Zone 700 mm (within +/- 2 °C)
Temperature Controller PID automatic control, 30 programmable segments, auto-tune function
Temperature Accuracy +/- 1 °C
Thermocouple Type K-type
Vacuum Capability 50 mtorr (mechanical pump); 10^-5 torr (molecular pump)
Flange Configuration Includes 1" flange for center tube and special triple-layer flange set
Standard Ports 3/8" barbed hose fittings (upgradable to KF25 or Swagelok)
Regulatory Compliance CE Certified; All electrical parts UL/MET/CSA certified

Why Choose TU-C26

Choosing this specialized tube furnace means investing in a solution specifically tailored for the niche requirements of high-magnetic field research. Unlike standard furnaces that utilize magnetic alloys or lack sufficient thermal insulation for confined magnet bores, this system is built from the ground up with SS316L and a triple-layer jacket. This ensures that your research environment remains stable, your magnets remain cold, and your data remains untainted by stray magnetic influences.

The engineering excellence of this unit is evident in its thermal precision and robust vacuum performance. With a 700mm constant temperature zone and the ability to reach high vacuum levels, it provides a highly stable platform for the most sensitive material annealing processes. The integration of UL-certified components and CE compliance underscores our commitment to safety and international standards in laboratory equipment manufacturing.

Furthermore, our ability to provide customized tube sizes and specialized fitting ports allows this furnace to be integrated into existing experimental setups with minimal modification. We provide comprehensive technical support and documentation to ensure seamless installation and operation. For a detailed quotation or to discuss your specific high-field research requirements, please contact our technical sales team today.

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