Rotary Furnace
1100°C Dual Zone Rotary Tube Furnace with Automatic Feeding and Collection System for Continuous Powder Processing
Item Number: TU-X02
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Product Overview



This high-performance thermal processing system represents a significant advancement in continuous materials synthesis, specifically engineered for the precise sintering and analysis of granular and powder-based materials. By combining dual-zone temperature control with a dynamic rotary environment, this equipment provides a seamless workflow from automated raw material input to the collection of processed products. The system is designed to eliminate the limitations of static batch processing, offering a level of throughput and heating uniformity that is essential for modern material science and high-end industrial R&D. Whether operating under a controlled atmosphere or high vacuum, the furnace ensures that every particle is exposed to consistent thermal conditions, which is crucial for achieving high-purity results in sensitive chemical reactions and phase transformations.
Primarily utilized in universities, national research institutes, and private industrial laboratories, this system excels in the demanding fields of energy storage and advanced metallurgy. It is the ideal solution for processing lithium-ion battery cathode and anode materials, as well as non-corrosive powders that require exact temperature profiles and meticulous handling. The industrial-grade construction allows for researchers to scale their chemical processes from initial development to pilot-scale production with high confidence. By automating the feeding and collection stages, the equipment minimizes human intervention, reduces the risk of contamination, and significantly increases the repeatability of complex multi-stage thermal cycles.
Reliability and operational safety are the cornerstones of this unit's design architecture. Built with a double-shell casing and secondary cooling fans, the external chassis remains safe to the touch even during prolonged high-temperature operations. The high-purity alumina fibrous insulation is selected for its superior energy-saving properties and thermal stability, preventing degradation during rapid heating and cooling cycles. This equipment is not merely a tool but a robust platform designed to withstand the rigors of intensive laboratory use, ensuring that researchers can focus on their material innovations without concern for hardware failure or inconsistent thermal performance. Every component, from the DC-driven rotation motor to the PID microprocessor, is integrated to deliver a stable, predictable, and high-performance sintering environment.
Key Features
- Advanced Dual-Zone Precision Heating: Featuring two independently controlled heating zones, this furnace allows for the creation of complex temperature gradients or extended uniform heat zones. Each zone is managed by an individual digital PID controller, ensuring that specific thermal profiles required for multi-stage chemical reactions can be maintained with an accuracy of ±1°C.
- Continuous Automatic Feed and Collection: This system is equipped with a high-capacity 500 ml automatic feeder and a 50 ml KF40 stainless steel collection tank. The integrated auger-driven feeder supports adjustable feeding rates from 3 to 60 ml/min, enabling precise control over material dwell time and throughput for industrial-grade continuous processing.
- Dynamic Rotary Mixing with Internal Vanes: The special-shaped quartz tube is designed with internal lifting vanes that cause powders to tumble and mix continuously as the tube rotates. This dynamic motion prevents powder stacking, eliminates internal temperature gradients, and ensures that the reaction atmosphere reaches every particle surface for complete and uniform sintering.
- Variable Speed and Tilting Capabilities: To control the flow rate and residence time of materials, the furnace features a DC motor-driven rotation (2–10 rpm) and an adjustable tilting mechanism (-5° to +20°). This flexibility allows operators to fine-tune the system according to the unique flow characteristics of various granular or crystalline materials.
- Atmosphere and Vacuum Optimized Sealing: Utilizing a sophisticated ferrofluid seal assembly and quick-clamp flanges, the equipment maintains vacuum integrity even during active rotation. This allows for sensitive materials to be processed under high vacuum up to 1000°C or under inert gas atmospheres, preventing oxidation and ensuring material purity.
- Rapid Cooling Split-Cover Design: The hinged split-cover construction facilitates easy access to the quartz tube for maintenance and enables significantly faster cooling between runs. Combined with the triple cooling fan system, this feature reduces downtime and allows for higher daily laboratory throughput.
- Sophisticated 50-Segment PID Control: The dual controllers offer a 50-segment programmable interface, allowing for complex heating, soaking, and cooling ramps. This automation ensures that once a recipe is established, the system delivers identical thermal conditions every time, which is critical for the graphitization and structural ordering of advanced catalysts.
- Industrial Resilience and Safety: The unit is housed in a robust double-shell casing with integrated safety features including mechanical pressure gauges, ball-valve gas outlets, and over-temperature alarms. The design ensures high thermal efficiency and complies with rigorous international safety standards, making it suitable for high-stakes industrial environments.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Battery Material Synthesis | Sintering of lithium-ion cathode and anode materials such as LFP, NMC, and graphite-based powders. | Ensures phase purity and uniform particle morphology through continuous dynamic mixing and precise zone control. |
| Catalyst Carbonization | Thermal treatment of nitrogen-doped carbon and metal-organic frameworks (MOFs) at 1100°C. | Facilitates the formation of stable Co-N cluster sites, significantly enhancing electrical conductivity and methanol tolerance. |
| Ceramic Powder Calcination | Processing of high-performance ceramic precursors and oxides under controlled vacuum or atmospheric conditions. | Elimination of static hot spots leads to higher structural uniformity and consistent particle size distribution in the final product. |
| Nanomaterial Coating | Chemical vapor deposition (CVD) processes where powders are coated with thin films while tumbling. | High surface area exposure during rotation ensures 360-degree coating uniformity for each individual particle or granule. |
| Granular Metallurgy | Reduction and sintering of metallic powders and master alloys in a continuous flow environment. | Precise control over residence time via tilting and rotation speed allows for high-throughput production of high-purity alloys. |
| Solid-State Reactions | Synthesis of complex inorganic compounds where gas-solid interaction is required for reaction completion. | Constant agitation in the rotary tube maximizes the reaction interface, accelerating synthesis times and improving yield. |
| Phosphorus Material R&D | Processing of high-purity phosphoric compounds under inert gas to prevent degradation and moisture sensitivity. | Hermetic ferrofluid seals and vacuum-tight flanges protect sensitive precursors from environmental contamination during heating. |
Technical Specifications
| Feature | Specification Details (Model: TU-X02) |
|---|---|
| Model Number | TU-X02 |
| Furnace Construction | Double shell casing with three integrated cooling fans; high-purity Alumina fibrous insulation. |
| Working Voltage | Single-phase AC 110V ±5%, 50/60Hz |
| Power Output | 2 kW |
| Thermocouple Type | Type K |
| Max Operating Temp | 1100°C (≤ 60 min) |
| Continuous Operating Temp | 1050°C (Air) / 1000°C (Vacuum) |
| Heating Rate | Recommended ≤ 10°C/min |
| Temperature Accuracy | ±1°C |
| Heating Zone Length | Dual Zones: 200 mm each |
| Tilting Angle | Adjustable from -5° to +20° |
| Rotary Tube Dimensions | φ30 mm (ends) × φ50 mm (center) × 700 mm length |
| Tube Material | Special-shaped Quartz tube with internal lifting vanes |
| Rotation Speed | 2 – 10 rpm (adjustable via DC motor) |
| Max Material Capacity | Approximately 30 ml per batch in the active zone |
| Automatic Feeder | 500 ml volume, adjustable feeding rate 3–60 ml/min, Stainless steel auger |
| Collection System | 50 ml stainless steel KF40 collection tank |
| Vacuum Sealing | Ferrofluid seal assembly with KF40 quick-clamp flanges and silicone O-rings |
| Gas Handling | φ6.35mm gas inlet with needle valve, mechanical gauge (-0.1 to 0.15 MPa), KF25 vacuum port |
| Temperature Controller | Dual digital PID controllers, 50-segment programmable; MET certified |
| Dimensions (Closed) | 1600 mm × 640 mm × 1300 mm (L × D × H) |
| Dimensions (Opened) | 1600 mm × 640 mm × 1450 mm (L × D × H) |
| Software (Optional) | Labview-based control system with data logging and wireless remote management |
| Certification | CE Certified; NRTL (UL61010) or CSA available upon request |
Why Choose TU-X02
- Superior Thermal Uniformity: The combination of dual-zone heating and dynamic rotary action eliminates the common issue of temperature gradients in powder processing, ensuring that 100% of your material undergoes the exact same thermal cycle.
- Precision Engineering and Build Quality: Constructed with high-purity alumina fiber and double-shell cooling, this system is designed for high-duty cycles in demanding industrial environments, ensuring years of consistent performance with minimal maintenance.
- Automated Workflow for Higher ROI: By integrating professional feeding and collection mechanics, the system significantly reduces labor costs and human error, transforming labor-intensive batch processing into a streamlined, high-yield operation.
- Versatile Atmosphere Control: Whether your process requires high vacuum, inert gas purging, or reactive atmospheres, the ferrofluid seal technology provides the most reliable vacuum-tight environment available for rotating systems.
- Global Compliance and Support: This equipment is CE certified and can be configured for NRTL or CSA standards, backed by our technical team's responsive support and extensive expertise in high-temperature material science equipment.
To discuss how this advanced dual-zone rotary system can optimize your powder processing workflow or to request a customized configuration quote, please contact our engineering specialists today.
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