Dual Zone Tube Furnace 1100C with 11 Inch Quartz Tube and Vacuum Flanges for 8 Inch Wafer Processing

Tube Furnace

Dual Zone Tube Furnace 1100C with 11 Inch Quartz Tube and Vacuum Flanges for 8 Inch Wafer Processing

Item Number: TU-32

Max Temperature: 1100°C Tube Diameter: 11" (279mm) O.D. Heating Zone Length: 24" (600mm) Total
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Product Overview

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This high-performance dual zone tube furnace is a sophisticated thermal processing system designed for advanced material research and industrial R&D. Featuring an exceptionally large 11-inch O.D. fused quartz tube, the equipment provides a spacious heating environment suitable for large-scale samples and semiconductor wafers up to 8 inches in diameter. The dual-zone configuration allows for the creation of precise thermal gradients or a wider constant temperature zone, offering researchers unparalleled flexibility in managing complex heat treatment profiles. By integrating high-purity alumina fibrous insulation, this system ensures maximum energy efficiency and rapid thermal response times.

The equipment is specifically engineered for high-purity applications, including the sintering of new material samples and the annealing of semiconductor wafers under vacuum or controlled gas atmospheres. Target industries range from semiconductor manufacturing and metallurgy to nanotechnology and renewable energy research. The large-diameter processing chamber allows for higher throughput and the accommodation of specialized crucibles and boats, making it an ideal choice for laboratories transitioning from small-scale experimentation to pilot-scale development. Its robust vacuum capabilities and gas handling features facilitate precise control over the chemical environment during critical processing stages.

Reliability and consistency are the hallmarks of this unit's design. Built to withstand demanding industrial conditions, the system utilizes high-precision digital controllers and durable NiCrAl resistance wire heating elements to maintain stable performance over extended periods. The inclusion of water-cooled stainless steel flanges protects the integrity of vacuum seals, ensuring a leak-free environment even during high-temperature cycles. This commitment to engineering excellence ensures that every process, from basic calcination to advanced chemical vapor deposition, is performed with repeatable, high-accuracy results that professional researchers can depend on.

Key Features

  • Precision Dual-Zone Temperature Control: The system features two independently controlled heating zones, each 300mm in length, managed by high-precision PID digital controllers. This allows for the establishment of stable thermal gradients or a combined 300mm constant temperature zone with ±1°C accuracy, essential for processes like TMD nanoribbon growth.
  • Extra-Large 11-Inch Quartz Chamber: Equipped with a massive 279mm O.D. fused quartz tube, this furnace accommodates large-format samples, including standard 8-inch semiconductor wafers. The high-purity quartz material provides excellent thermal shock resistance and chemical inertness, ensuring a contaminant-free environment.
  • Advanced Hinged Vacuum Flanges: The stainless steel vacuum flanges feature a hinged design for effortless sample loading and unloading. Integrated water-cooling channels in the double-layer flange structure effectively protect the O-ring seals, maintaining vacuum integrity during sustained operation at temperatures up to 1100°C.
  • High-Efficiency Thermal Insulation: Utilizing high-purity alumina fibrous insulation, the equipment minimizes heat loss and reduces energy consumption. This lightweight, high-performance insulation also enables faster heating and cooling rates, optimizing the overall cycle time for laboratory throughput.
  • Robust Heating Elements and Safety: Long-life NiCrAl resistance wire heating elements provide consistent heat distribution. For operator and equipment safety, a secondary temperature monitor is included to protect against over-temperature conditions and broken thermocouples, providing peace of mind during unattended operation.
  • Integrated Gas and Vacuum Porting: The system includes a mechanical vacuum gauge, two stainless steel needle valves, and a KF25 vacuum port. This comprehensive fitting suite allows for precise atmosphere management, supporting vacuum levels from 10-2 torr with mechanical pumps up to 10-4 torr with turbomolecular systems.
  • Programmable Heat Treatment Profiles: Both temperature controllers support 30 programmable segments, allowing users to automate complex ramp, soak, and cool-down sequences. This ensures high reproducibility across multiple batches, which is critical for standardized research and industrial quality control.
  • Computer Interface and Data Logging: The equipment is compatible with specialized Labview-based control software, enabling researchers to edit temperature profiles, manage recipes, and record real-time data on a PC for thorough post-process analysis and documentation.

Applications

Application Description Key Benefit
Semiconductor Wafer Annealing Thermal processing of large-format wafers (up to 8") to repair crystal defects or activate dopants. Superior uniformity across the entire wafer surface area.
TMD Nanoribbon Growth Utilizing dual zones to independently control chalcogen vapor pressure and substrate reaction temperature. Precise control over nanoribbon width and growth kinetics via supersaturation.
Catalytic Pyrolysis High-temperature decomposition of organic materials, such as waste tires, under controlled atmospheres. Prevention of localized overheating and excessive carbonization via stable gradients.
Material Sintering Consolidation of powder materials into dense solids for structural or electronic ceramics research. Consistent density and grain structure achieved through ±1°C accuracy.
Chemical Vapor Deposition (CVD) Precise deposition of thin films using specialized gas mixtures and large-diameter processing tubes. Accommodates large substrates and high-volume gas flow for scalable research.
Vacuum Heat Treatment Stress relieving or hardening of metal components in an oxygen-free environment. Eliminates oxidation and surface contamination during high-temp cycles.

Technical Specifications

Parameter Specifications for TU-32
Model Number TU-32
Tube Material High-purity Fused Quartz
Tube Dimensions 279mm O.D x 269mm I.D x 1000mm Length (11" x 10.6" x 40")
Max. Temperature 1100°C (< 60 min, under inert gas)
Continuous Temperature 400°C - 1000°C (under vacuum or flowing gas)
Optional Temperature 1150°C (with upgraded GE 214 quartz tube)
Heating Zones Dual zones: 300mm (12") each; 600mm (24") total
Constant Temp Zone 300mm at center (±1°C) when zones are set identically
Heating Rate Max. 20°C / min
Temperature Accuracy ±1°C
Temperature Controller Two PID digital controllers with 30 programmable segments
Thermocouple Dual K-type (12" x 1/4" Dia Grounded Probe)
Heating Element NiCrAl Resistance Wire
Input Voltage 208 - 240V AC, Single Phase
Power Rating 8 kW
Vacuum Flanges Double-layer stainless steel, water-cooled, hinged type
Vacuum Ports KF25 port, 1/4" hose fittings, two needle valves
Vacuum Limit 10-2 torr (mechanical pump) / 10-4 torr (turbo pump)
Cooling Requirement Water flow ≥ 10L/min, Temp < 25ºC, Pressure > 25 PSI
Compliance CE Certified (NRTL/CSA available upon request)

Why Choose Us

  • Industrial-Grade Reliability: Engineered with high-durability resistance wires and advanced fibrous insulation, this system is designed for long-term operational consistency in demanding research environments.
  • Large-Scale Capability: The 11-inch diameter tube is a rare offering in laboratory-scale furnaces, providing the necessary volume for 8-inch wafer processing and large material batches without requiring industrial-sized equipment.
  • Precision Thermal Management: Independent dual-zone control provides the thermal flexibility required for complex chemical vapor deposition and nanostructure growth, ensuring the highest level of experimental control.
  • Robust Safety and Protection: Built-in secondary temperature monitoring and water-cooled flange systems safeguard your laboratory assets and ensure the longevity of high-vacuum seals.
  • Comprehensive Integration: From Labview software compatibility to customizable gas mixing and vacuum station options, this furnace serves as a complete, expandable platform for your thermal processing needs.

For more information on the TU-32 dual zone furnace or to receive a custom quote tailored to your specific vacuum and gas handling requirements, please contact our technical sales team today.

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