Tube Furnace
Four Zone Tube Furnace 1100C with 600mm Large Diameter Quartz Tube and Vacuum Flanges
Item Number: TU-47
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Product Overview


This high-performance four-zone tube furnace represents a pinnacle in thermal processing engineering, specifically designed to accommodate large-scale material samples and 8-inch wafers. By utilizing a massive 600mm (24") diameter high-purity quartz tube, the system provides an expansive environment for specialized heat treatments that require both volume and precision. The core value of this equipment lies in its multi-zone configuration, which allows for intricate control over thermal gradients, making it an indispensable tool for advanced chemical vapor deposition (CVD), annealing, and sintering processes where uniformity is paramount.
Targeted at industrial R&D centers and material science laboratories, this equipment excels in handling diverse atmospheric conditions. Whether operating under a high vacuum or specific protective gas environments, the system maintains its integrity through robust engineering. The dual-layer steel casing with integrated air cooling ensures that while the internal chamber reaches high temperatures, the external surface remains safe for operators, facilitating a productive and secure laboratory environment. This unit is optimized for the synthesis of new materials, offering researchers the flexibility to simulate complex industrial manufacturing conditions at a bench-scale or pilot-scale level.
Reliability is at the forefront of this design, featuring a refractory fibrous alumina insulation liner that maximizes energy efficiency and thermal stability. The system is built to withstand demanding industrial duty cycles, providing consistent performance across thousands of hours of operation. With its ability to handle structural ordering and graphitization of advanced carbon materials, the equipment serves as a dependable backbone for projects involving catalyst development, semiconductor research, and metallurgical testing. This system is not merely a furnace but a comprehensive thermal solution for high-stakes material innovation.
Key Features
- Four-Zone Independent Temperature Management: The system features four distinct heating zones, each 300 mm in length, providing a total heated length of 1200 mm. This configuration allows for the creation of precise thermal gradients or an exceptionally long constant temperature zone of up to 1100 mm, ensuring unmatched processing flexibility for long substrates or high-volume batches.
- Extra-Large Diameter Quartz Processing Tube: Equipped with a 600 mm (24") OD high-purity quartz tube, this unit is specifically designed for processing large-format materials, such as 8-inch wafers. The quartz material provides excellent thermal shock resistance and chemical inertness, maintaining a contamination-free environment for high-purity sintering and annealing.
- Precision Microprocessor PID Control: Each zone is governed by a dedicated digital controller featuring 30-segment programmable cycles and self-tuning functions. The microprocessor-based PID logic prevents temperature overshooting and maintains a steady-state accuracy of ±1°C, which is critical for sensitive material transformations and repeatable results.
- Advanced Multi-Stage Vacuum Sealing: The system includes a pair of water-cooled stainless steel hinged flanges designed for rapid access and superior sealing. Utilizing silicon O-rings and integrated KF40 ports, the furnace can achieve vacuum levels as low as 10-5 torr when paired with secondary turbomolecular pumps, facilitating ultra-clean processing conditions.
- Industrial-Grade Heating Elements: Utilizing high-quality NiCrAl resistance wire heating elements, the furnace achieves a maximum heating temperature of 1150°C. These elements are chosen for their durability and consistent heat release, ensuring long-term reliability even when subjected to frequent thermal cycling.
- Integrated Safety and Cooling Systems: The double-layer steel casing is engineered with internal air cooling to keep the external surface temperature below 70°C. This design protects laboratory personnel and prevents ambient heat buildup, while the inclusion of a recirculating water chiller for the flanges protects seals during high-temperature runs.
- Comprehensive Monitoring and Calibration: The unit is equipped with four K-type thermocouples for real-time monitoring of each zone. The flanges include specialized ports for secondary calibration thermocouples, allowing users to verify internal temperatures and ensure the highest standards of process validation and quality control.
- High-Efficiency Refractory Insulation: High-quality fibrous alumina insulation liners minimize heat loss and power consumption. This energy-efficient design combined with ceramic tube blocks effectively contains radiation, focusing thermal energy into the processing zone rather than the surrounding environment.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Semiconductor Wafer Annealing | Post-deposition thermal treatment of 8-inch silicon or compound semiconductor wafers. | Improves crystal structure and electrical properties with high uniformity. |
| Large-Scale CVD Processes | Chemical Vapor Deposition of thin films or nanomaterials across large surface areas. | Precise control over gas dynamics and temperature gradients for high-purity coatings. |
| Carbon Graphitization | Thermal treatment of nitrogen-doped carbon at 1100°C to enhance electrical conductivity. | Optimizes Co-N cluster stability and catalyst performance for fuel cell applications. |
| Multi-Zone Sintering | Heat treatment of ceramic or metallic samples requiring specific heating and cooling ramps. | Prevents cracking and structural defects through controlled thermal distribution. |
| Atmospheric Research | Heat treatment under controlled inert or reactive gases (N2, Ar, H2) with flow control. | Enables simulation of complex industrial chemical environments in a laboratory setting. |
| Powder Metallurgy | Vacuum sintering of advanced alloy powders to achieve high density and purity. | Removes oxides and prevents contamination during the consolidation process. |
| Materials Aging Studies | Sustained high-temperature testing of industrial components to evaluate thermal fatigue. | Provides consistent, long-term thermal stability for reliable degradation data. |
Technical Specifications
| Feature | Specification Details (Model TU-47) |
|---|---|
| Heating Zone Length | Total 1200 mm (4 Zones x 300 mm per zone) |
| Constant Temperature Zone | 1000 mm (±3°C) or 1100 mm (±5°C) longitude direction |
| Maximum Temperature | 1150°C (< 1 hour) |
| Continuous Working Temp | 200°C to 1100°C |
| Heating/Cooling Rate | ≤ 5°C/min |
| Temperature Accuracy | ± 1°C |
| Temperature Uniformity | ± 3°C along the cross-section |
| Quartz Tube Dimensions | OD 600 mm x ID 590 mm x L 1500 mm (24" Diameter) |
| Furnace Structure | Double-layer steel casing with air cooling; Surface < 70°C |
| Insulation Liner | Refractory fibrous alumina insulation |
| Heating Element | NiCrAl Resistance Wire |
| Controllers | Four digital PID controllers, 30-segment programmable |
| Thermocouple Type | Four K-type thermocouples (one per zone) |
| Vacuum Level | 10-2 torr (mechanical pump); up to 10-5 torr (turbopump) |
| Flange Type | Water-cooled SS hinged flanges with KF40 and 1/4" ports |
| Chiller Requirement | Included 16L/min recirculating water chiller |
| Power Consumption | ~50 KW |
| Rated Voltage | Three Phase, 220V AC, 50/60 Hz |
| Compliance | CE Certified (NRTL/CSA available upon request) |
| Gas Flow Limitation | < 200 SCCM to reduce thermal shock |
| Pressure Limit | < 0.2 bar / 3 psi |
Why Choose Us
- Superior Thermal Uniformity: The four-zone architecture provides an exceptionally large constant temperature zone, making this unit the premier choice for large-format substrates and bulk processing where thermal consistency determines product quality.
- Robust Industrial Build: Engineered with heavy-duty steel, water-cooled stainless steel flanges, and high-efficiency alumina insulation, this system is designed for the rigors of continuous R&D and pilot production environments.
- Exceptional Vacuum Integrity: The hinged flange design combined with high-speed turbopump compatibility ensures that researchers can achieve and maintain the ultra-clean atmospheres necessary for high-purity chemical vapor deposition.
- Precision Engineering and Support: Each system is calibrated to strict standards and supported by a suite of available accessories, including gas delivery systems, hydrogen leak detectors, and calibration kits to ensure long-term operational accuracy.
- Customizable High-Capacity Processing: With its unique 600mm tube diameter, this furnace fills the gap between standard laboratory units and industrial production kilns, offering a professional-grade solution for scaling up advanced material research.
Our technical team is ready to assist you in configuring the ideal thermal solution for your specific processing requirements. Contact us today for a technical consultation or a formal quotation.
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