Tube Furnace
1200C Three Zone Split Vertical Tube Furnace 4 Inch Quartz Tube Stainless Steel Vacuum Flanges
Item Number: TU-C13
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Product Overview



This vertical thermal processing system represents a sophisticated solution for material science laboratories and industrial R&D facilities requiring precise atmosphere control and rapid temperature cycling. By integrating a split-shell design with a vertical orientation, the equipment facilitates efficient sample loading and unloading while optimizing workspace in high-traffic research environments. Its primary value proposition lies in the ability to maintain extreme thermal stability across three independent heating zones, allowing for the creation of precise temperature gradients or extended isothermal regions required for advanced crystal growth and chemical vapor deposition processes.
Targeting sectors such as aerospace engineering, semiconductor development, and solid-state chemistry, this system provides the versatility needed for complex heat treatment recipes. The combination of high-purity quartz tubing and robust vacuum sealing ensures that sensitive materials are processed without contamination. Whether performing rapid quenching tests or steady-state sintering, the unit delivers the repeatability and accuracy essential for generating high-quality research data in both academic and industrial settings.
Constructed with industrial-grade components and a focus on long-term operational reliability, the furnace is designed to withstand the rigors of continuous high-temperature service. The split casing allows for easy maintenance and fast cooling, while the integrated heavy-duty mobile base ensures that the entire system can be repositioned safely within a facility. This investment in premium engineering translates to consistent performance, minimizing downtime and maximizing the throughput of critical research projects where precision is non-negotiable.
Key Features
- Independent Three-Zone Heating Control: The system features three distinct heating zones, each 300mm in length, which can be controlled independently to create custom thermal gradients. This setup is crucial for applications like Bridgman crystal growth or ensuring a highly uniform temperature profile across a 600mm constant heating zone when zones are synchronized.
- Precision Split-Shell Design: The furnace body is engineered with a split-shell configuration that opens lengthwise. This allows users to easily insert or remove the process tube and facilitates rapid cooling of the sample after high-temperature cycles without the need for complex disassembly of vacuum connections.
- Advanced Vacuum Sealing System: Equipped with dual stainless steel vacuum flanges, the unit includes high-quality valves and a vacuum gauge. The top flange features an integrated hook ring, designed specifically for hanging crucibles or samples for quenching experiments, ensuring vertical stability during the heat treatment process.
- High-Purity Fused Quartz Reaction Tube: The standard 4-inch diameter quartz tube provides excellent thermal shock resistance and chemical inertness. This material is ideal for maintaining a high-purity environment under vacuum or flowing gas, allowing researchers to monitor reaction progress visually through the transparent tube.
- Sophisticated PID Temperature Regulation: The MET-certified controller provides 30 programmable segments for precise management of heating rates, cooling rates, and dwell times. Accuracy is maintained within ±1°C, supported by built-in PID auto-tune functions and broken thermocouple protection for unattended safety.
- Robust Thermal Insulation: Utilizing high-quality fibrous insulation, the system is designed for maximum energy efficiency. This material minimizes heat loss and ensures that the exterior casing remains at a safe temperature even during sustained operation at the 1200°C maximum threshold.
- Integrated Safety Features: The system includes over-temperature protection and alarms as standard, allowing for safe overnight operation. The double-layered steel casing incorporates an air-cooling fan system to keep the outer surface temperature below 55°C, protecting lab personnel and surrounding equipment.
- Heavy-Duty Mobile Integration: The entire furnace unit is mounted on a heavy-duty, industrial mobile cart. This allows for easy relocation of the equipment within a facility while providing a stable, vibration-damped platform for sensitive experimental setups.
- Digital Communication Capability: Featuring an RS485 communications port, the furnace can be integrated with external computer systems. This enables remote monitoring, data logging of heating profiles, and automation of complex thermal recipes through Labview-based software environments.
- Expandable Atmosphere Control: Standard 1/4" barbed needle valve fittings allow for the introduction of protective gases. The system can be upgraded with Swagelok fittings or KF25 adapters to accommodate high-vacuum pumps and precise mass flow controllers for CVD applications.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Quenching Research | Rapid cooling of metallic or ceramic samples from high temperatures via vertical hanging and quick-release mechanisms. | Precise control over phase transformation kinetics and microstructural evolution. |
| Chemical Vapor Deposition | Synthesis of thin films and nanomaterials by delivering precursor gases into the controlled thermal environment of the quartz tube. | Excellent uniformity across the large 600mm constant heating zone for consistent film thickness. |
| Crystal Growth | Utilization of the three-zone control to establish precise temperature gradients required for Bridgman or vapor transport methods. | High-resolution spatial temperature control necessary for single-crystal quality. |
| Semiconductor Doping | High-temperature diffusion of dopants into silicon wafers or other semiconductor substrates within a high-purity quartz environment. | Minimal contamination and repeatable thermal cycles for batch uniformity. |
| Catalyst Synthesis | Calcination and reduction of catalytic materials under controlled atmospheres (flowing nitrogen, argon, or forming gas). | High-purity gas flow management and accurate dwell time control for active site preservation. |
| Sintering of Ceramics | Consolidation of powder compacts into dense ceramic components at temperatures up to 1200°C under vacuum. | Elimination of porosities through effective atmospheric removal and precise ramp-rate control. |
| Phase Diagram Studies | Determination of thermal stability and phase transition points in material mixtures using steady-state isothermal holds. | Long-term temperature stability (±1°C) for reliable material characterization data. |
| High-Vacuum Processing | Heat treatment of sensitive alloys that require pressures down to 0.1 torr to prevent oxidation or nitridation. | Reliable vacuum integrity provided by CNC-machined stainless steel flanges and O-ring seals. |
Technical Specifications
| Specification Category | Parameter Details (TU-C13) |
|---|---|
| Model Identifier | TU-C13 |
| Furnace Structure | Double layer steel casing with forced air cooling; < 55°C surface temperature |
| Insulation | High-purity fibrous ceramic insulation for energy efficiency |
| Power Rating | 7 KW |
| Voltage Requirements | AC 208-240V Single Phase, 50/60 Hz |
| Maximum Temperature | 1200°C |
| Continuous Operating Temp | 1100°C |
| Max Heating Rate | ≤ 20°C /min |
| Tube Material | High-purity Fused Quartz |
| Tube Dimensions | OD: 102mm; ID: 94mm; Length: 1540mm (4 inch diameter) |
| Standard Package | Includes one 4" quartz tube; Optional 2", 3", and 5" adapters available |
| Heating Zone Config | Three zones (3x 300mm) for a total heating length of 900mm |
| Constant Heat Zone | 600mm (when all three zones are set to identical temperatures) |
| Temp Controller | MET certified; 30 programmable segments; PID Auto-Tune; RS485 Port |
| Temperature Accuracy | ± 1ºC |
| Vacuum Sealing | Two stainless steel flanges; integrated gauge, valves, and top-flange hook |
| Fitting Ports | Standard 1/4’’ Barbed fittings with needle valves |
| Vacuum Level | 0.1 torr (up to 10-4 torr with optional digital gauge and high-vac pumps) |
| Heating Elements | Fe-Cr-Al Alloy doped by Mo for enhanced longevity |
| Compliance | CE Certified; NRTL/CSA available upon request |
| Vacuum Limitations | Safe for use under vacuum up to 1000°C; internal pressure < 0.2 bars |
| Gas Flow Limit | Recommended < 200 SCCM to reduce thermal shock to the quartz tube |
Why Choose TU-C13
- Engineered for Precision: The independent three-zone control allows for unprecedented flexibility in thermal profiling, making the system ideal for complex material synthesis that requires both uniformity and gradients.
- Uncompromising Build Quality: Featuring Fe-Cr-Al alloy elements doped with Molybdenum and high-purity fibrous insulation, the system is built to provide years of reliable service in demanding industrial and research environments.
- Enhanced Safety and Ease of Use: The combination of a split-vertical design for rapid access and a double-layered air-cooled casing ensures that the unit is both productive for researchers and safe for the laboratory environment.
- Versatile Atmosphere Control: With its stainless steel vacuum flanges and the ability to upgrade to high-vacuum fittings, this equipment handles vacuum, inert gas, and reactive gas environments with total integrity.
- Certified Reliability: All units are CE certified and built to rigorous engineering standards, providing peace of mind for procurement teams and compliance officers in regulated industries.
Contact our technical sales team today to request a quotation or to discuss a customized thermal solution tailored to your specific material science requirements.
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