Tube Furnace
1100°C Three Zone Tube Furnace with 8.5 to 11 Inch OD Quartz Tube and Vacuum Flanges for Large Wafer Processing
Item Number: TU-39
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Product Overview


This high-capacity thermal processing system is engineered specifically for large-scale semiconductor wafer processing, advanced material research, and industrial-grade heat treatments. By integrating a massive three-zone heating configuration with large-diameter quartz tubing, the equipment provides an expansive processing volume without sacrificing the thermal precision required for sensitive chemical vapor deposition (CVD) or annealing cycles. The unit is designed to operate continuously at 1100°C, providing a robust platform for high-throughput laboratory environments and pilot production lines that demand repeatable results and high-purity atmospheres.
Targeting the semiconductor, aerospace, and energy storage sectors, this equipment excels in applications ranging from wafer diffusion to the structural optimization of catalyst materials. The three-zone design allows for the creation of precise thermal gradients or a significantly extended uniform heating zone, which is critical for processing larger substrates or multiple samples simultaneously. This versatility makes the system a cornerstone for facilities focused on scaling up material synthesis from benchtop experiments to industrial-ready prototypes.
Built with reliability as a priority, the furnace utilizes a double-layer steel casing and advanced fibrous alumina insulation to ensure operational safety and energy efficiency. The inclusion of hermetic, water-cooled stainless steel flanges allows for high-vacuum operations and controlled atmosphere processing, ensuring that even the most demanding metallurgical or chemical processes are contained within a stable and clean environment. This system represents a significant investment in durability, offering long-term performance under rigorous R&D schedules.
Key Features
- Independent Three-Zone Thermal Control: The system features three distinct heating zones, each measuring 300 mm in length, controlled by individual PID programmable controllers. This allows for a total heating length of 900 mm (approximately 35.4"), providing the operator with the flexibility to establish a 600 mm constant temperature zone or complex thermal gradients required for specialized vapor transport processes.
- Large-Format Quartz Integration: Capable of housing quartz tubes ranging from 8.5" (216 mm) to 11" (279 mm) in outer diameter, the furnace accommodates large-scale wafer boats and oversized industrial components. This high-volume capacity is rare in laboratory-scale tube furnaces, bridging the gap between small-scale research and full industrial production.
- High-Performance FeCrAl Heating Elements: High-quality iron-chromium-aluminum (FeCrAl) resistance wires are strategically embedded within the refractory fibrous alumina insulation. These elements are chosen for their exceptional resistance to oxidation and thermal fatigue, ensuring a long service life even when cycled frequently to maximum operating temperatures.
- Advanced Hermetic Vacuum Sealing: The furnace is equipped with a pair of hinged-style, water-cooled stainless steel flanges. These flanges feature integrated vacuum gauges, needle valves, and KF40 ports, enabling the system to achieve vacuum levels as low as 5e-2 torr with a mechanical pump, or higher with optional turbo-pumping systems.
- Superior Thermal Insulation and Safety: A double-layer steel casing with integrated air cooling ensures that the outer surface temperature remains below 70°C during peak operation. The use of high-purity alumina fiber insulation minimizes heat loss and reduces power consumption, while maintaining high heating and cooling rates of up to 10°C/min.
- Precision PID Instrumentation: Each zone is monitored by dual K-type thermocouples and managed by a 30-segment programmable controller with +/- 1°C accuracy. This level of control is essential for preventing thermal overshoot and ensuring the integrity of delicate substrates during long-duration annealing or diffusion steps.
- Robust Gas Handling Capabilities: The flange assembly includes stainless steel needle valves and quick-connect ports, facilitating the introduction of inert or reactive gases. This makes the system ideal for atmosphere-controlled processes where gas flow and pressure must be strictly maintained.
- Optimized for Wafer Processing: The design supports optional quartz baffle blocks and specialized wafer boats (up to 8" for larger tube variants), making it a turnkey solution for semiconductor annealing, oxidation, and diffusion processes.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Semiconductor Wafer Annealing | High-temperature treatment of silicon or compound semiconductor wafers to repair crystal defects and activate dopants. | Superior uniformity across large diameters (up to 11") ensures consistent electrical properties. |
| Catalyst Material Synthesis | Facilitates structural ordering and graphitization of nitrogen-doped carbon and Co-N cluster sites at 1100°C. | Enhanced stability and uniform distribution of active sites for improved limiting current values. |
| Atmospheric CVD | Chemical Vapor Deposition of thin films onto various substrates using controlled gas flows and high heat. | Precise three-zone control allows for the necessary temperature gradients to drive precursor reactions. |
| Large-Scale Powder Calcination | Thermal decomposition of materials or removal of volatile fractions from large batches of industrial powders. | High-volume quartz tube allows for significant throughput per batch compared to standard lab furnaces. |
| Solid State Battery Research | Sintering of ceramic electrolytes and electrode materials under controlled vacuum or inert conditions. | Hermetic sealing prevents contamination and ensures high-purity material development. |
| Aerospace Material Testing | Subjecting advanced alloys and composites to high-temperature oxidative environments to simulate flight conditions. | Reliable 1100°C continuous operation provides the durability required for long-term fatigue testing. |
| Carbon Nanotube Growth | Large-scale synthesis of CNTs through thermal decomposition of hydrocarbon gases over catalyst substrates. | Extended uniform heating zone (600mm) maximizes the yield of high-quality nanotubes per run. |
Technical Specifications
| Parameter | TU-39-8.5 | TU-39-11 |
|---|---|---|
| Quartz Tube Dimensions | 216 O.D x 206 I.D x 1300mm L (8.5" x 8.1" x 51") | 279 O.D x 269 I.D x 1300mm L (11" x 10.6" x 51") |
| Max. Wafer Boat Size | 6" Wafer Boat | 8" Wafer Boat |
| Power Requirements | 208-240VAC, 1-Phase, 50/60 Hz, 40 A | 208-240VAC, 1-Phase, 50/60 Hz, 40 A |
| Maximum Temperature | 1200°C (< 1 hour) | 1200°C (< 1 hour) |
| Continuous Working Temp | 1100°C | 1100°C |
| Heating Length | 900 mm (Total) / 300mm + 300mm + 300mm | 900 mm (Total) / 300mm + 300mm + 300mm |
| Uniform Zone Length | 600 mm (+/- 3°C @ 800°C) | 600 mm (+/- 3°C @ 800°C) |
| Heating/Cooling Rate | Max. 10°C/min | Max. 10°C/min |
| Temperature Control | Three PID Controllers, 30 Segments | Three PID Controllers, 30 Segments |
| Control Accuracy | +/- 1°C | +/- 1°C |
| Thermocouple Type | Dual K-type per zone | Dual K-type per zone |
| Vacuum Flanges | Water-cooled stainless steel (hinged) | Water-cooled stainless steel (hinged) |
| Vacuum Level | < 5e-2 torr (Mechanical Pump) | < 5e-2 torr (Mechanical Pump) |
| Max. Pressure | ≤ 3 psig | ≤ 3 psig |
| Shell Construction | Double-layer steel with air cooling | Double-layer steel with air cooling |
| Chilled Water Requirement | >16 L/min, 5-30 °C, <80 psig | >16 L/min, 5-30 °C, <80 psig |
Why Choose This Three-Zone Tube Furnace
- Industrial-Grade Throughput: The rare combination of 11" OD tube capacity and a 900mm heating length allows researchers to process large substrates or high volumes of material that typically require industrial-scale equipment.
- Precision Engineering: With triple-zone PID control and +/- 1°C accuracy, this system provides the thermal stability necessary for reproducible material science and semiconductor fabrication.
- Advanced Safety and Stability: The double-walled casing design and water-cooled flanges ensure a safe laboratory environment and protect the system's internal seals during high-temperature, long-duration cycles.
- High-Vacuum Integrity: Engineered with hinged hermetic flanges and KF40 ports, the system is designed for high-purity processes requiring vacuum levels as low as 5e-2 torr, making it suitable for cleanroom environments.
- Customizable Control Options: Beyond the standard PID configuration, this unit can be upgraded with Eurotherm 3000 series controllers and Labview-based software for advanced recipe editing and automated data logging.
Our technical team is ready to assist with custom configurations or specific process requirements to ensure this system meets your exact R&D or production needs. Contact us today for a detailed quote or to discuss your thermal processing specifications.
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