Tube Furnace
1200C Max Four Zone Split Tube Furnace with Optional Large Diameter Quartz Tubes
Item Number: TU-46
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Product Overview


This high-performance thermal processing system is engineered to meet the rigorous demands of industrial R&D and advanced material science. Designed as a large-scale, split-able four-zone furnace, it provides exceptional flexibility for researchers and production engineers who require precise temperature gradients or extended uniform zones. The split-cover architecture allows for easy access to the reaction chamber, facilitating the rapid loading and unloading of samples or the integration of complex internal assemblies without dismantling the entire tube setup. By combining a 1200°C maximum operating temperature with specialized large-diameter quartz tube options, this system is uniquely positioned to handle high-volume processing and large-format substrates that standard laboratory furnaces cannot accommodate.
The equipment excels in applications requiring controlled atmospheres and high-vacuum environments. Whether tasks involve the synthesis of advanced ceramics, the annealing of semiconductor wafers, or the sintering of metallic powders, this unit delivers the thermal stability necessary for reproducible results. Its four-zone configuration is optimized to create a massive 36-inch uniform temperature zone, a critical requirement for scaling up laboratory processes to pilot-plant levels. Target industries include semiconductor manufacturing, aerospace material development, energy storage research, and high-purity chemical processing, where consistency and reliability are non-negotiable.
Built with heavy-duty industrial components, this system reflects a commitment to long-term operational excellence. The chassis features a double-layered steel construction integrated with dual cooling fans to maintain a safe, low-touch skin temperature during high-temp cycles. Reliability is further bolstered by the inclusion of high-purity fibrous alumina insulation, which minimizes heat loss and improves energy efficiency. For procurement teams and lab managers, this furnace represents a premium investment in thermal infrastructure, balancing high-throughput capabilities with the precision of a high-end laboratory instrument.
Key Features
- Independently Controlled Four-Zone Design: The equipment features four distinct heating zones totaling 47 inches in length, allowing for the creation of precise thermal gradients or a remarkably long 36-inch uniform zone within ±5°C. This level of control is essential for complex CVD processes and long-sample annealing.
- Pneumatic Split-Cover Operation: To ensure ease of use and operator safety, the top cover is driven by two heavy-duty pneumatic cylinders. This mechanical assist allows for smooth opening and closing of the split furnace, facilitating rapid cooling and easy tube replacement even in high-throughput environments.
- Large-Scale Chamber Versatility: This system supports optional high-purity quartz tubes with internal diameters of 8, 10, or 14 inches. This versatility enables the processing of large wafers, bulky components, or high volumes of smaller samples in a single thermal cycle.
- Precision PID Temperature Regulation: Equipped with four programmable digital controllers, the unit offers 30 segments for managing heating rates, cooling rates, and dwell times. The ±1°C accuracy ensures that even the most sensitive materials are processed within strict tolerances.
- Industrial-Grade Cooling and Insulation: The double-layer steel case is paired with twin cooling fans to ensure the exterior remains safe for contact. High-purity fibrous alumina insulation provides excellent thermal retention while significantly reducing power consumption during extended runs.
- Advanced Vacuum Sealing Technology: The unit includes a pair of stainless steel 304 vacuum flanges featuring double high-temperature silicone O-rings and integrated water-cooling jackets. This ensures seal integrity and longevity, even when operating at the systems upper temperature limits.
- Comprehensive Safety Systems: Built-in overheating and broken thermocouple protection, along with an over-temperature alarm, allow for confident, unattended operation. The system is designed to shut down safely in the event of a thermal excursion, protecting both the equipment and the valuable samples within.
- High-Performance Thermal Elements: Fe-Cr-Al alloy heating elements doped with Mo provide rapid heating and excellent resistance to oxidation. These elements are strategically positioned to provide balanced radiant heat across the entire circumference of the process tube.
- Ready-to-Integrate Digital Communication: An RS485 communication port and specialized software are included as standard. This allows users to monitor and control the furnace via a laptop, enabling data logging and remote recipe management for standardized industrial workflows.
- Optimized Thermal Buffer Blocks: Buffer-type quartz disc thermal blocks are included to maintain the internal cleanliness of the chamber and prevent heat radiation from damaging the flange seals, further extending the service life of the consumable components.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Semiconductor Wafer Annealing | High-temperature treatment of silicon or SiC wafers to repair crystal defects and activate dopants. | Large 14" ID capacity allows for batch processing of multiple wafers simultaneously. |
| Chemical Vapor Deposition (CVD) | Used as the thermal reactor for synthesizing 2D materials, carbon nanotubes, or thin-film coatings. | Four-zone control allows for precise precursor evaporation and deposition temperature gradients. |
| Sintering of Technical Ceramics | High-heat processing of ceramic powders to create dense, high-strength components for aerospace and medical use. | Exceptional thermal uniformity (±5°C) across 36 inches prevents warping and internal stresses. |
| Atmospheric Diffusion | Introducing dopants into solid materials under controlled gas environments like Argon, Nitrogen, or Hydrogen. | Double-silicone O-ring flanges ensure high vacuum or high-purity atmosphere integrity throughout. |
| Aerospace Alloy Aging | Precise heat treatment of specialty alloys used in turbine blades and structural airframe components. | Pneumatic split-top allows for rapid quenching or immediate access to samples post-cycle. |
| Energy Storage Research | Calcination and sintering of cathode/anode materials for next-generation lithium-ion and solid-state batteries. | Robust PLC-ready software integration facilitates the logging of critical production data. |
| Large-Format Glass Stress Relieving | Annealing large glass or quartz components to remove internal stressors after fabrication or welding. | The 47-inch total heating length accommodates oversized industrial glass workpieces effortlessly. |
Technical Specifications
| Feature | Specification Details (Model TU-46) |
|---|---|
| Heating Zone Length | Total: 1200mm (47"); 4 Zones @ 300mm (11.8") each |
| Uniform Temperature Zone | 914mm (36") within ±5ºC |
| Max Operating Temp | 1200°C (≤ 1 hour) |
| Continuous Operating Temp | 1100°C |
| Vacuum Temperature Limit | < 1000°C (under high vacuum conditions) |
| Max Heating Rate | 10°C / minute |
| Tube Options (ID x OD x L) | 8.1" ID x 8.5" OD x 60" L (206 x 216 x 1524 mm) 10.6" ID x 11.0" OD x 51" L (269 x 279 x 1295 mm) 14.6" ID x 15.0" OD x 73" L (371 x 381 x 1860 mm) |
| Power Requirements | AC 208-240V Three Phase, 50/60 Hz (50A breaker required) |
| Max Power Consumption | 24 KW |
| Vacuum Integrity | 10^-2 Torr (Mechanical Pump); 10^-5 Torr (Turbopump) |
| Sealing System | SS 304 flanges with water-cooling jackets and dual silicone O-rings |
| Control Interface | 4 sets of 30-segment PID digital controllers (MET/CE Certified) |
| Accuracy | ±1ºC (Standard PID); Optional Eurotherm ±0.1ºC |
| Gas Management | Two needle valves and vacuum pressure gauge installed on flanges |
| Compliance | CE Certified; NRTL (UL61010) or CSA available upon request |
Why Choose TU-46
Investing in this four-zone system ensures your laboratory or production facility is equipped with a tool designed for the highest levels of thermal precision and operational longevity. Unlike standard single-zone furnaces, the four-zone architecture provides the granular control needed to eliminate "cold spots" over large sample areas, ensuring that batch consistency is maintained even when working at the 14-inch diameter scale. This capability is pivotal for reducing material waste and improving the yield of high-value industrial processes.
The engineering of this unit prioritizes ruggedness without sacrificing the finesse required for material research. From the pneumatic lift system that reduces operator fatigue to the water-cooled vacuum flanges that protect sensitive seals, every component is selected for its ability to withstand continuous use in demanding environments. Our manufacturing process complies with stringent CE and MET standards, providing procurement teams with the documentation and safety assurance required for modern industrial facilities.
Furthermore, we understand that every research process has unique requirements. We offer extensive customization for this furnace, including the integration of Eurotherm high-precision controllers, mass flow controllers for multi-gas mixing, and various vacuum pump configurations ranging from mechanical to turbo-molecular systems. This flexibility ensures that the equipment can evolve alongside your research objectives.
Choosing this furnace means partnering with a brand dedicated to technical excellence and responsive support. Our team provides comprehensive guidance on installation, maintenance, and process optimization to ensure you achieve your thermal goals. Contact us today to discuss your specific large-diameter tube requirements or to request a detailed quotation for a customized configuration.
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