High Temperature Rocking Tube Furnace 1700°C Alumina Processing Tube with Precision Oscillation for Material Synthesis

Rotary Furnace

High Temperature Rocking Tube Furnace 1700°C Alumina Processing Tube with Precision Oscillation for Material Synthesis

Item Number: TU-X19

Maximum Temperature: 1700°C Rocking Range: +/- 45° Adjustable Processing Tube: 60mm OD x 800mm Alumina
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Product Overview

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This high-temperature rocking tube furnace represents a pinnacle in thermal processing engineering, designed specifically for material science researchers and industrial laboratories requiring superior composition uniformity. By combining a maximum operating temperature of 1700°C with a precision-controlled mechanical rocking mechanism, the equipment facilitates the processing of powders, granules, and heterogeneous mixtures under controlled atmospheres. The core value of this system lies in its ability to prevent material clumping and sintering through continuous physical agitation, ensuring that every particle is exposed to the same thermal and gas conditions throughout the cycle.

Optimized for demanding R&D environments, the unit is frequently utilized in the development of advanced ceramics, battery electrodes, and catalyst materials. The rocking motion, adjustable up to +/- 45 degrees, creates a fluid-like movement within the alumina processing tube, which is essential for achieving a truly homogenous product. This mechanical action, paired with high-purity alumina insulation and a robust heating array, allows for repeatable results in complex solid-state reactions and calcination processes across various high-tech sectors including aerospace, renewable energy, and metallurgy.

Reliability is at the heart of the design. Built with industrial-grade components and a dual-layer cooling architecture, this furnace ensures stable performance during long-duration thermal cycles. The integration of 1800-grade molybdenum disilicide (MoSi2) heating elements provides the thermal power necessary for rapid ramping and stable soaking, while the protective casing maintains a safe external environment. Procurement teams and lead researchers can rely on this equipment for consistent, high-purity processing in the most critical material development phases.

Key Features

  • Precision Rocking Mechanism: The integrated 150W DC gear motor enables a controlled swing of the furnace body from +/- 45 degrees, promoting mechanical mixing and preventing local hotspots or material agglomeration during the heating cycle.
  • High-Performance MoSi2 Heating Elements: Utilizing 1800-grade Molybdenum Disilicide elements, the system reliably reaches 1700°C, providing the thermal energy required for advanced material synthesis and sintering processes.
  • Advanced PID Temperature Control: A 30-segment programmable controller offers +/- 1°C accuracy, allowing for complex ramping, soaking, and cooling profiles to be executed with extreme precision and repeatability.
  • Dual-Layer Air-Cooled Casing: The heavy-duty steel exterior features built-in air cooling channels that maintain a surface temperature below 60°C, ensuring operator safety and long-term structural integrity of the electronics.
  • High-Purity Alumina Processing Environment: The unit includes a 60mm OD high-purity alumina tube and fibrous ceramic blocks, which provide an inert and thermally stable environment for processing high-purity powders and chemical compounds.
  • Versatile Atmosphere Control: Equipped with dual stainless steel vacuum flanges and 1/4" barbed fittings, the system supports both high-vacuum operations and controlled gas purging for oxidation-sensitive materials.
  • Dynamic Speed and Frequency Adjustment: Users can fine-tune the rocking frequency from 0.1 to 1 cycle per minute and adjust the internal drive speed, allowing for the optimization of agitation based on material density and particle size.
  • Comprehensive Safety Systems: Built-in over-temperature and thermocouple failure alarms automatically cut power to the heating elements, protecting both the equipment and the processed materials from accidental thermal excursions.
  • Expandable Controller Options: While the standard PID controller is highly capable, the system can be upgraded to Eurotherm 3000 series units for researchers requiring +/- 0.1°C accuracy and advanced data logging capabilities.
  • Robust Vacuum Integrity: The precision-machined KF25 vacuum ports and high-quality seals allow the system to achieve vacuum levels as low as 50 m-torr with standard mechanical pumps, or 10^-5 torr with optional turbo-molecular systems.

Applications

Application Description Key Benefit
Battery Material Synthesis Calcination of cathode and anode powders for lithium-ion and solid-state batteries. Enhanced ion conductivity through uniform particle size and composition.
Catalyst Development Thermal activation and reduction of catalytic substrates under specific gas atmospheres. Maximized surface area and active site distribution due to constant material movement.
Technical Ceramics Sintering of high-performance ceramic powders and precursors at temperatures up to 1700°C. Elimination of density gradients within the processed material batch.
Powder Metallurgy Heat treatment and reduction of metal powders for additive manufacturing and specialized alloys. Prevention of particle fusion during high-temperature processing phases.
Solid-State Reactions Synthesis of complex oxides and phosphors through long-duration high-temperature soaking. Faster reaction kinetics and improved phase purity via mechanical agitation.
Carbon Nanotube Growth Chemical Vapor Deposition (CVD) processes where rocking helps distribute catalysts. Higher yield and more consistent tube morphology across the substrate.
Phosphor Production High-temperature firing of rare-earth doped materials for lighting and display technologies. Superior color uniformity and luminescence through homogenous doping.
Gemstone Treatment Controlled heating and atmosphere cycles for the enhancement of mineral and gemstone properties. Precise control over oxidation states and thermal gradients for high-value results.

Technical Specifications

Specification Category Parameter Details Value (TU-X19)
Model Identifier Product Item Number TU-X19
Thermal Performance Maximum Operating Temperature 1700°C (< 2 hours)
Continuous Working Temperature 1600°C
Recommended Heating Rate ≤ 10°C / min
Heating Architecture Heating Elements 1800 Grade MoSi2 Elements
Heating Zone Length 300 mm (12")
Constant Temperature Zone 80 mm (+/- 1°C)
Rocking Parameters Rocking Angle Adjustable up to +/- 45°
Rocking Frequency 0.1 - 1 time per minute
Drive Motor 150W Gear DC Motor
Adjustable Speed Range 10 - 70 RPM (Internal Drive)
Rocking Timer 1 - 1199 minutes or Continuous
Processing Tube Material High Purity Alumina (>99.5%)
Dimensions 54 mm (I.D) x 60 mm (O.D) x 800 mm (L)
Radiation Protection Fibrous ceramic tube blocks included
Control System Controller Model FA-YD518P-AG (Eurotherm Optional)
Programming 30 segments (Ramping, Cooling, Dwelling)
Temperature Accuracy +/- 1°C (Standard) / +/- 0.1°C (Upgraded)
Communication Interface RS485 PC Port with included software
Atmosphere & Vacuum Flange Type Stainless Steel with Vacuum Gauge & Valves
Port Fittings 1/4" Barbed fittings; KF25 Vacuum Port
Achievable Vacuum 50 m-torr (Mechanical); 10^-5 torr (Turbopump)
Electrical Data Power Supply AC 208 - 240V, 50/60Hz, Single Phase
Power Rating 3.0 kW (Requires 20A Breaker)
Physical Build Cooling System Double-layer steel casing with air cooling
External Safety Case temperature remains < 60°C
Compliance CE Certified; NRTL/CSA optional

Why Choose High Temperature Rocking Tube Furnace

  • Unmatched Material Homogeneity: The precision rocking action is engineered to eliminate the thermal and concentration gradients common in static tube furnaces, providing a significant advantage for powder processing and solid-state synthesis.
  • Industrial-Grade Reliability: From the 1800-grade MoSi2 elements to the dual-layer cooled steel housing, every component of this system is selected for its ability to withstand the rigors of 24/7 industrial R&D environments.
  • Precision Control Infrastructure: With the ability to program 30 distinct segments and the option to upgrade to +/- 0.1°C Eurotherm controllers, researchers have total command over the most sensitive thermal profiles.
  • Customizable Processing Environment: Whether you require specific tube lengths, customized thermal blocks, or specialized flange fittings, our engineering team can adapt the system to meet your exact experimental requirements.
  • Proven Safety and Compliance: CE certification and the option for NRTL or CSA testing ensure that this equipment meets the highest global safety standards for laboratory and industrial installations.

Invest in a thermal processing solution that combines mechanical agitation with extreme high-temperature precision. Contact us today to discuss your specific application requirements or to request a customized quote for your facility.

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