Rotary Furnace
1100C High Pressure Rocking Tube Furnace with 2 Inch Super Alloy Processing Tube for Material Synthesis
Item Number: TU-X20
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Product Overview
This high-performance thermal processing system is engineered for advanced material science applications requiring the simultaneous application of high temperature, high pressure, and mechanical agitation. By integrating a three-zone heating architecture with a specialized rocking mechanism, the equipment ensures exceptional homogeneity during the melting of alloys or the synthesis of compounds that are prone to evaporation under standard atmospheric conditions. This makes it an indispensable tool for laboratories focusing on volatile material synthesis and specialized crystal growth.
Designed for rigorous industrial R&D environments, this system excels in processing materials under both inert gas and oxygen environments. The core of the equipment is a high-strength super-alloy processing tube capable of maintaining structural integrity at temperatures up to 1100ºC while under significant internal pressure. This unique combination of capabilities allows researchers to explore phase diagrams and material behaviors that are impossible to reach in conventional tube furnaces, providing a significant competitive advantage in advanced metallurgy and chemical engineering.
Reliability and consistency are the cornerstones of this equipment's design. Featuring a split-able furnace body for easy tube access and a separate control console for operator safety, the unit is built to withstand the demanding cycles of industrial heat treatment. The inclusion of high-precision PID controllers and a robust mechanical drive system ensures that every process is repeatable and documented, meeting the stringent quality standards required for modern material certification and pilot-scale production.
Key Features
- Nickel-Based Super-alloy Tube: The processing chamber is constructed from GH747 super-alloy, specifically selected for its superior creep resistance and oxidation stability at high temperatures, allowing for safe operation under high-pressure conditions.
- Precision Three-Zone Heating: The furnace involves three independently controlled heating zones, enabling the creation of precise thermal gradients or an extended constant temperature zone of 280 mm with ±1°C accuracy.
- Automated Rocking Mechanism: An integrated 150W DC gear motor facilitates a rocking angle of -30º to +90º, ensuring mechanical mixing of the melt and preventing sedimentation or segregation in complex alloy systems.
- High-Pressure Capability: Engineered for extreme environments, the system supports internal gas pressures up to 40 bar at lower temperatures and remains operational at 8 bar even at the 1100ºC peak limit.
- Advanced Thermal Regulation: Utilizing FA-YD518P-AG digital controllers, the system offers 30-segment programming with auto-tune functionality for precise ramping, dwelling, and cooling cycles.
- Separated Safety Control Unit: For enhanced operator protection, all pressure, temperature, and rocking parameters are managed via a remote touch-screen panel, isolating the user from the high-temperature zone.
- Dual Flange Integration: The inclusion of both high-pressure CF flanges with copper O-rings and constant-pressure KF adaptors provides flexibility for different sealing requirements and gas handling configurations.
- Integrated Gas Filtration: A core funnel filter and external cold trap protect the exhaust system and maintain high purity levels by capturing condensable vapors before they exit the processing zone.
- Robust Mechanical Stability: The rocking stage is built to support the furnace weight while maintaining smooth, adjustable frequency ranges from 0.1 to 1 time per minute for consistent processing.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Volatile Alloy Melting | Processing of alloys containing elements with high vapor pressures. | Prevents loss of alloying elements for precise composition control. |
| N-Doped Carbon R&D | High-pressure graphitization of nitrogen-doped carbon materials. | Enhances electrical conductivity and stability of catalytic sites. |
| Compound Synthesis | Solid-gas reactions at elevated pressures and temperatures. | Accelerates reaction kinetics and improves product yield in complex syntheses. |
| Materials Characterization | Stress-testing materials under simultaneous thermal and pressure loads. | Simulates extreme industrial environments for durability verification. |
| Crystal Growth | Controlled cooling of melts with continuous rocking agitation. | Promotes homogeneous crystal structures and reduces defect density. |
| Hydrothermal Mimicry | Simulating high-pressure geological or industrial chemical processes. | Allows for atmospheric and pressurized experimental flexibility in one unit. |
| Catalyst Optimization | Thermal treatment of catalysts to improve methanol tolerance. | Produces more stable and uniformly distributed active cluster sites. |
Technical Specifications
| Feature | Parameter | Specification for TU-X20 |
|---|---|---|
| Model Identifier | Item Number | TU-X20 |
| Heating Architecture | Configuration | Split-able furnace with 3 independent heating zones |
| Zone Length | Individual / Total | 150 mm per zone / 450 mm total length |
| Constant Temp. Zone | Precision Range | 280 mm (±1°C) |
| Max. Temperature | Peak Operating Limit | 1100°C (< 1 hour) |
| Continuous Temperature | Standard Working Limit | 1000°C |
| Heating Rate | Maximum Ramp | 10°C / minute |
| Processing Tube | Material & Dimensions | Ni-based Superalloy GH747; OD 60 x ID 52 x L 1000 mm |
| Pressure Tolerances | Pressure vs Temp | 40 bar (@800°C), 25 bar (@900°C), 12 bar (@1000°C), 8 bar (@1100°C) |
| Rocking Parameters | Angle / Frequency | -30º to +90º / 0.1 to 1 time/min adjustable |
| Drive System | Motor Power / Speed | 150W DC Gear Motor / 10 - 70 RPM display |
| Temperature Control | Controller Model | Three FA-YD518P-AG PID controllers (RS485 Included) |
| Power Supply | Voltage / Consumption | AC 208-240V, 50/60Hz; 4.2 KW |
| Gas Compatibility | Media | Inert gases or Oxygen (No Flammable/Hydrogen) |
| Flange Type | Sealing Method | CF Flanges with copper O-rings (High Pressure) |
| Filtration | Components | Core funnel filter and external Cold Trap |
| Compliance | Standards | CE Certified; NRTL (UL61010/CSA) available at request |
Why Choose TU-X20
- Superior Pressure-Temperature Performance: Built with premium GH747 super-alloy, this system safely bridges the gap between atmospheric heating and high-pressure chemical synthesis, allowing for experiments that standard quartz or ceramic tubes cannot support.
- Process Homogeneity: The precision-engineered rocking mechanism is a critical advantage for researchers needing to prevent settling in melts or ensure uniform gas-solid interactions throughout the processing cycle.
- Enhanced Process Safety: The remote control architecture and modular design isolate high-pressure and high-temperature risks from the operator, ensuring a secure laboratory environment for multi-user facilities.
- Versatile Gas Management: Equipped with dual flange options and advanced filtration, this system handles corrosive or condensable gases with ease, protecting the equipment and the surrounding laboratory environment.
- Industrial-Grade Reliability: From the high-torque gear motor to the precision PID temperature controllers, every component is selected for long-term operational consistency in demanding R&D cycles.
Engineered to meet the sophisticated requirements of modern material science, our 1100C rocking tube furnace represents a premium investment in your facility's research capabilities. Contact THERMUNITS today for a detailed technical consultation or a customized quote for your specific synthesis needs.
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