High Temperature 1700C Tube Furnace with 4 Inch OD Alumina Tube and Vacuum Sealing Flanges

Tube Furnace

High Temperature 1700C Tube Furnace with 4 Inch OD Alumina Tube and Vacuum Sealing Flanges

Item Number: TU-73

Max. Working Temperature: 1700 °C Heating Tube Material: 99.8% High-purity Alumina (4" OD) Temperature Control Accuracy: ± 1 °C (PID Programmable)
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Product Overview

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This high-temperature bench-top furnace system provides a versatile and robust solution for material science and chemical research laboratories requiring extreme thermal processing up to 1700ºC. Designed for precision and stability, the equipment is engineered to facilitate the sintering of advanced material samples under varied atmospheric conditions, including high vacuum and inert gas environments. The compact footprint and high-performance heating profile make it an essential tool for institutional and industrial RD centers focusing on ceramics, metallurgy, and semiconductor development.

Primary use cases for the system involve precisely controlled heat treatments where atmosphere purity is critical. By integrating high-purity alumina processing tubes with sophisticated sealing assemblies, this unit allows researchers to explore phase transformations, crystal growth, and chemical vapor deposition processes. The furnace's architecture is optimized for rapid thermal cycling and long-term temperature maintenance, ensuring that demanding experimental protocols are executed with repeatable accuracy.

Reliability is at the core of this thermal processing unit's design. Utilizing a double-layer steel casing with advanced air-cooling technology, the equipment maintains a safe touch-temperature even during peak operation. The integration of 1800-grade Molybdenum Disilicide (MoSi2) heating elements ensures longevity and consistent performance under high-temperature loads. Procurement teams can be confident in the system’s industrial-grade components and its ability to withstand the rigors of continuous high-heat scientific inquiry.

Key Features

  • Advanced 1800-Grade MoSi2 Heating Elements: The furnace utilizes eight high-specification Molybdenum Disilicide elements capable of withstanding temperatures beyond the system's operating limit, ensuring a large safety margin and extended component lifespan during 1700ºC cycles.
  • Precision Alumina Refractory Chamber: The internal heating zone is lined with high-purity alumina fiber insulation, which minimizes heat loss, improves thermal uniformity, and prevents contamination of sensitive samples during processing.
  • Dual-Layer Casing with Active Cooling: A heavy-duty steel outer shell with integrated cooling fans maintains the external surface temperature below 60ºC, protecting lab personnel and surrounding equipment while enhancing the longevity of internal electronics.
  • Sophisticated PID Temperature Control: This system features a programmable digital controller providing ±1ºC accuracy. Users can configure up to 30 process segments for complex ramping, soaking, and cooling protocols, supported by phase-angle fired SCR power control.
  • Integrated Vacuum Sealing Flange Kit: The equipment includes a complete stainless steel sealing assembly with a KF25 vacuum port and 1/4" gas pipe adaptors, enabling immediate transition between vacuum, inert gas, and ambient atmospheres.
  • Safety Monitoring and Over-Temperature Protection: A built-in over-temperature alarm and automatic shut-off mechanism allow for unsupervised operation, providing peace of mind during long-duration sintering or annealing processes.
  • High-Purity American-Made Alumina Tube: For the 100mm OD variant, the system incorporates a chemical-resistant alumina tube designed for superior thermal shock resistance and chemical inertness under extreme heat.
  • Versatile Atmospheric Control: Utilizing two stainless steel needle valves and a dial vacuum gauge, the system provides granular control over gas input and vacuum levels, essential for sensitive chemical vapor deposition (CVD) workflows.
  • Phase-Angle Fired SCR Technology: Unlike standard solid-state relays, the silicon-controlled rectifier (SCR) power control provides a smoother power delivery to the elements, reducing thermal stress and increasing temperature precision.
  • Scalable Digital Communication: The unit is equipped with an RS485 communication port, allowing for PC-based monitoring and data logging, facilitating strict QC compliance and experimental documentation.

Applications

Application Description Key Benefit
Advanced Ceramics Sintering Consolidation of ceramic powders into dense bodies at temperatures up to 1700ºC. High thermal uniformity ensures consistent material density and mechanical properties.
Powder Metallurgy Sintering of metal powders and alloys under vacuum or inert atmospheres to prevent oxidation. Precise atmosphere control preserves the purity of the metal matrix.
Crystal Growth Controlled thermal gradients for the synthesis and growth of single crystals for optics and electronics. Stable temperature soaking minimizes internal stress in growing crystals.
Chemical Vapor Deposition (CVD) Deposition of thin films onto substrates through gaseous chemical reactions. Seamless integration with gas mixing stations and vacuum pumps.
Annealing & Stress Relieving Heat treatment of semiconductor wafers or metallurgical samples to alter physical properties. Programmable cooling rates prevent thermal shock and micro-cracking.
Catalyst Testing Evaluating the thermal stability and efficiency of catalysts under high-heat flow conditions. Robust corrosion resistance of the alumina tube handles varied chemical vapours.
Battery Material Research Synthesis of cathode and anode materials requiring specific atmospheric calcination. Reliable repeatability for comparative research studies.

Technical Specifications

Core Furnace Parameters (Item: TU-73)

Parameter Specification Details
Heating Zone Length 457 mm (18")
Constant Temperature Zone 150 mm (6")
Maximum Working Temperature 1700 ºC (< 1 hour duration)
Continuous Working Temperature 800 ºC to 1600 ºC
Heating / Cooling Rate Maximum 10 ºC/min
Temperature Accuracy ± 1 ºC (Optional ± 0.1ºC with premium controllers)
Power Rating Maximum 7 kW
Input Voltage Single Phase, 220V AC, 50/60 Hz (40 A breaker required)
Heating Elements 8 pcs Super 1800ºC grade MoSi2 (30 x 330 mm)
Thermocouple Type B-Type Thermal Couple

Processing Tube & Sealing (TU-73 Variants)

Component Specification Details
Tube Material 99.8% High purity Al2O3 ceramic (Made in the US)
Standard Tube Dimensions 101 mm OD × 92 mm ID × 1200 mm L
Optional Tube Diameters 60 mm OD, 80 mm OD
Vacuum Sealing Double silicone high-temperature O-rings with SS flanges
Fitting Ports 1/4" Barbed fittings (Optional Swagelok or KF25)
Vacuum Level (Mechanical) 50 mtorr achieved with standard mechanical pump
Vacuum Level (Turbo) 10^-5 torr achievable with molecular pump station
Maximum Internal Pressure < 0.02 MPa (Absolute pressure)

Controller & Safety Compliance

Feature Details
Standard Controller PID automatic control with 30 programmable segments
SCR Interface Phase angle fired SCR for high-precision power modulation
Optional Controller Eurotherm 3000 Series (1 program, 24 segments)
Communications RS485 Port (PC control module optional)
Structure Double-layer steel casing with dual air-cooling fans
Cooling Limit Case temperature remains < 60 ºC during operation
Compliance CE Certified (NRTL/CSA available upon request)

Why Choose High Temperature 1700C Tube Furnace

  • Unrivaled Thermal Precision: By employing Super 1800ºC grade MoSi2 elements and phase-angle fired SCR control, the system delivers temperature stability that exceeds industry standards, ensuring that sensitive research outcomes are never compromised by thermal fluctuations.
  • Robust Vacuum Engineering: Unlike many standard tube furnaces, our sealing assembly features double silicone O-rings and integrated needle valves as standard, providing a turn-key solution for researchers working under high-vacuum or strictly controlled atmospheres.
  • Enhanced Operational Safety: The combination of active cooling fans, a double-walled casing, and built-in over-temperature alarms creates a secure laboratory environment, allowing high-heat processes to run alongside other analytical activities without risk.
  • Superior Material Integrity: We utilize 99.8% high-purity alumina tubes and refractory chambers to ensure that no contaminants leach into your samples at 1700ºC, a critical requirement for high-purity chemical and semiconductor research.
  • Modular and Expandable Design: With options for PC-control integration, mass flow meter gas stations, and high-vacuum turbo pumping units, this equipment can evolve alongside your research needs, protecting your long-term capital investment.

Our engineering team is ready to discuss your specific process requirements, whether you need custom flange configurations or specialized control software integration. Contact us today to receive a technical consultation or a formal quotation for your laboratory upgrade.

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