High Temperature Three Zone Split Tube Furnace 1200C Max 35.4 Inch Heating Length 8 Inch ID Tube

Tube Furnace

High Temperature Three Zone Split Tube Furnace 1200C Max 35.4 Inch Heating Length 8 Inch ID Tube

Item Number: TU-38

Maximum Temperature: 1200°C Total Heating Zone Length: 35.4" (900mm) Processing Tube ID: 8.1" (206mm)
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Product Overview

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This high-performance thermal processing system is engineered for advanced material science applications requiring precise temperature gradients and exceptional thermal uniformity. By utilizing a three-zone heating configuration and a split-case design, the equipment provides researchers and industrial engineers with the flexibility to manage complex heat treatment cycles. The system is specifically optimized for high-temperature operations up to 1200°C, offering a robust platform for both atmospheric and vacuum-based processes. Its large 8-inch internal diameter tube accommodates substantial samples, making it an ideal choice for pilot-scale production and rigorous R&D workflows.

Primarily utilized in semiconductor research, metallurgy, and advanced ceramics, this unit excels in environments where precision and repeatability are non-negotiable. Whether performing chemical vapor deposition (CVD), sintering, or annealing, the equipment ensures that the sample environment remains stable and uncontaminated. Target industries include aerospace manufacturing, electronics development, and academic material science laboratories. The three independent heating zones allow for the creation of customized thermal profiles, which is critical for processes such as gradient crystallization or the synthesis of 2D materials like molybdenum disulfide.

Reliability is at the core of this system's design. Constructed with a double-layer steel case and integrated cooling fans, the equipment maintains a low exterior surface temperature even during prolonged high-temperature runs. The use of high-purity fibrous alumina insulation maximizes energy efficiency while ensuring rapid heating and cooling response times. B2B procurement teams can rely on this system for consistent performance under demanding industrial conditions, backed by professional-grade PID control and integrated safety mechanisms that allow for unattended operation with full confidence.

Key Features

  • Independent Three-Zone Thermal Management: The heating chamber is divided into three 11.8-inch sections, totaling a 35.4-inch heating length. Each zone is governed by its own digital controller, enabling the system to achieve a 12-inch uniform temperature zone within +/- 2ºC or create specific thermal gradients required for specialized material growth.
  • Precision Split-Case Architecture: The hinged furnace body allows for easy access to the processing tube and internal chamber. This design facilitates rapid tube replacement, simplified sample loading, and the ability to utilize pre-assembled experimental setups without the need to slide long tubes through fixed heating elements.
  • High-Purity Alumina Insulation: Engineered with energy-saving fibrous alumina, the insulation layer minimizes heat loss and improves the overall thermal response of the furnace. This material choice ensures a clean environment and prevents sample contamination from refractory particulates.
  • Advanced PID Temperature Control: Three MET and CE-certified digital controllers provide 30 programmable segments for precise regulation of heating rates, cooling rates, and dwell times. The system maintains a temperature accuracy of +/- 1ºC, ensuring repeatable results across multiple batches.
  • High-Vacuum and Gas Atmosphere Compatibility: The system includes heavy-duty stainless steel 304 vacuum flanges with double high-temperature silicone O-rings and water-cooling jackets. It is capable of achieving vacuum levels down to 10-5 torr when paired with a turbopump, supporting clean thermal processing in inert or reactive gas environments.
  • Integrated Safety and Protection Systems: A split-cover interlock protection system automatically cuts power when the furnace is opened. Additionally, the unit features built-in overheating and broken thermocouple protection, along with audible and visual alarms for over-temperature conditions.
  • Robust Heating Elements: High-quality K-type thermocouples and strategically placed heating elements ensure efficient energy transfer to the quartz tube, allowing for a maximum heating rate of 20°C per minute while maintaining the integrity of the thermal profile.
  • Scalable Digital Communication: Each controller is equipped with an RS485 communications port, allowing for optional PC-based data logging and remote operation. This scalability is essential for industrial environments where data traceability is a requirement for quality control.

Applications

Application Description Key Benefit
2D Material Synthesis Used for the synthesis of Ta and Nb-doped MoS2 as documented in ACS Nano research. Enables precise edge structure tailoring for electrocatalytic applications.
Diffusion Annealing High-temperature (1000°C+) homogenization of Fe-Ni-Cu alloys or semiconductor wafers. Eliminates diffusion rate deviations through superior three-zone uniformity.
CVD / PECVD Serving as the main heating unit for Chemical Vapor Deposition of graphene or carbon nanotubes. Provides a stable temperature environment over a long path for precursor reaction.
Sintering Ceramics Processing of advanced technical ceramics and oxide materials in controlled atmospheres. High-purity insulation prevents contamination during critical firing stages.
Thermal Gradient Growth Creating specific temperature slopes for single crystal growth or vapor transport. Independent zone control allows for fine-tuning of the thermal slope across the tube.
Oxidation Studies Analyzing the high-temperature oxidation behavior of alloys under air or oxygen. Consistent temperature control across large samples ensures reliable corrosion data.
Material Degassing Removal of trapped gases from bulk materials under high vacuum conditions. High-capacity 8-inch tube and vacuum sealing allow for high-throughput degassing.
Phase Transformation Investigating the phase transition points of experimental industrial alloys. Accurate PID control ensures precise identification of transformation temperatures.

Technical Specifications

Specification Category Parameter TU-38 Detailed Specification
Model Identification Item Number TU-38
Furnace Structure Housing Double-layer steel case with dual cooling fans
Insulation High-purity fibrous alumina (energy-saving)
Safety Feature Split cover with interlock protection
Electrical Data Power Requirement AC 208-240V, Three-phase, 50/60 Hz
Max Power Consumption 10 KW
Circuit Protection 50A breaker required
Heating Performance Max Heating Temperature 1200°C
Continuous Working Temp 1100°C (1000°C under vacuum)
Max Heating Rate 20°C / min
Zone Configuration Total Heating Length 900mm (35.4")
Individual Zone Length 300mm (11.8") per zone
Uniform Zone 300mm (12") within +/- 2ºC
Tube & Flanges Quartz Tube Dimensions 216mm OD x 206mm ID x 1524mm L (8.5" x 8.1" x 60")
Sealing Type SS 304 Vacuum Flanges with water cooling jacket
Fitting Ports KF-40D Adaptor, 2 needle valves, pressure gauge
Vacuum Level 10-2 torr (mechanical pump) to 10-5 torr (turbopump)
Temperature Control Controller Type 3x Digital PID Controllers (MET/CE Certified)
Programming Segments 30 programmable segments per controller
Accuracy +/- 1ºC
Communication RS485 Port
Compliance Certifications CE Certified (UL61010/CSA available upon request)

Why Choose This Three-Zone Split Tube Furnace

Investing in this three-zone split tube furnace represents a commitment to high-precision engineering and operational longevity. Unlike standard single-zone furnaces, this system provides the ability to stretch the "sweet spot" of temperature uniformity, which is critical when processing long samples or scaling up laboratory experiments to pilot production. The independent control over three distinct segments allows users to compensate for heat loss at the tube ends, resulting in a more predictable and stable thermal environment.

The structural integrity of the equipment is designed for the rigors of industrial research. From the double-layer steel casing that protects operators from high temperatures to the high-purity alumina insulation that prevents thermal bridging, every component is selected for durability. The split-furnace design not only improves ergonomics but also reduces downtime during sample turnover and tube maintenance, providing a significant advantage in high-utilization laboratory settings.

Furthermore, the versatility of the vacuum and gas delivery interface makes this a future-proof investment. Whether your current project requires a simple air atmosphere or a complex high-vacuum environment with reactive gas flow, this system is equipped to handle the transition with ease. Backed by industry-leading certifications and a proven track record in high-impact scientific publications, this furnace is the reliable choice for facilities that cannot afford to compromise on data accuracy or equipment uptime.

Our engineering team is available to assist with custom configurations, including integrated mass flow controllers or high-vacuum pumping stations tailored to your specific research parameters. Contact us today to receive a technical consultation and a formal quotation for your thermal processing requirements.

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