Small Vacuum Molybdenum Wire Sintering Furnace

Vacuum Sintering Furnace

Small Vacuum Molybdenum Wire Sintering Furnace

Item Number: TU-SJA

Rated Temperature: 0–1200°C Cold Limit Vacuum: 6.67 × 10⁻³ Pa Workspace Dimensions: Φ60 × 60 mm
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Product Overview

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This compact vacuum sintering furnace is engineered for precision high-temperature processing in laboratory and R&D environments. Featuring molybdenum wire heating elements and a high-integrity vacuum chamber, it provides contamination-free sintering for a wide range of advanced materials. The unit’s bottom-loading configuration and integrated cooling system simplify operation, while the rugged construction ensures long-term reliability.

Primary applications include sintering of technical ceramics such as alumina, zirconia, and silicon carbide, as well as hardmetal alloys and cermets. It also supports metal annealing, brazing, and degassing under high vacuum, and quartz dehydroxylation for optical and semiconductor uses. Its broad capability makes it an indispensable tool for materials science labs, universities, and industrial R&D centers.

Built with precision components and rigorous quality control, this furnace delivers consistent results even under extreme conditions. Advanced PID control maintains temperature stability, and the vacuum system achieves low ultimate pressures essential for high-purity processing. User-friendly automation, data logging, and a modular design ensure reproducibility and ease of maintenance, meeting the needs of modern research environments.

Key Features

  • Compact Integrated Design with Mobility: The furnace’s space-saving architecture consolidates the vacuum chamber, heater, controls, and pumping system into a single robust enclosure. Built-in heavy-duty swivel casters with locking brakes enable smooth movement and secure positioning, ideal for laboratories where equipment must be shared or reconfigured frequently.
  • Bottom Lift Loading Mechanism: A motorized ball-screw lift gently raises the hearth platform into the heating zone, ensuring smooth and repeatable sample placement. This design eliminates the need for manual reaching into the hot chamber, improving safety and ergonomics while accommodating taller crucibles or complex fixtures.
  • Advanced Touchscreen PLC Control: A high-resolution color touchscreen provides real-time visualization of temperature, vacuum level, and process status. The PLC controller supports multi-segment temperature and pressure profiles with ramp/soak programming, allowing precise execution of complex thermal cycles.
  • Extensive Process Storage and Recall: The controller memory can store up to 50 custom sintering recipes, each with configurable parameters. Operators can easily create, edit, copy, and delete programs directly on the screen or transfer them via USB for backup and remote editing, drastically reducing setup time and transcription errors.
  • Real-Time Data Logging and Export: Continuous data capture of temperature, vacuum, and time stamps with user-defined logging intervals. Data is stored on an internal flash drive and can be exported as CSV files for analysis, reporting, and compliance with laboratory documentation standards.
  • High-Performance Graphite Heating Element: The heating assembly features a robust graphite element capable of sustaining temperatures above 2300°C, surrounded by molybdenum wire insulation for excellent heat distribution. This design offers rapid heating rates, low thermal mass, and long service life even under aggressive cycling conditions.
  • Precise Temperature Control: Closed-loop PID temperature regulation with a dedicated thermocouple achieves control accuracy of ±1°C over the entire operating range. This stability is critical for achieving uniform material densification and minimizing thermal gradients that cause cracking or warping in sensitive parts.
  • Built-In Closed-Loop Water Chiller: An integrated water chiller maintains constant cooling water temperature, protecting critical seals and vacuum pump components. This self-contained system avoids the need for facility chilled water lines and ensures reliable cooling during extended high-temperature runs.
  • Versatile Atmosphere Management: The vacuum system includes a two-stage rotary vane pump and a high-vacuum diffusion pump to achieve ultimate pressures in the 10⁻³ Pa range. A mass flow controller–based gas inlet permits precise backfill of argon, nitrogen, or forming gas up to 0.05 MPa, enabling controlled sintering atmospheres.
  • Safety and Diagnostics: Comprehensive safety features include over-temperature alarm, cooling water flow interlock, vacuum gauge interlock, and emergency stop. Fault conditions are displayed in plain text on the touchscreen, facilitating rapid troubleshooting by operators.

Applications

Application Description Key Benefit
Ceramic Seals and Components Sintering Sintering of ceramic sealing rings, insulators, and structural parts from alumina, zirconia, or silicon carbide. Vacuum atmosphere removes binders cleanly and prevents oxidation, resulting in fully dense components with excellent mechanical properties. Achieves high hardness, wear resistance, and dimensional accuracy critical for demanding seal applications.
Hardmetal Tooling Sintering Vacuum sintering of tungsten carbide–cobalt hardmetal grades for cutting tools, dies, and wear parts. The controlled atmosphere prevents cobalt evaporation and ensures uniform binder phase distribution. Enhances fracture toughness and hardness, leading to extended tool life and consistent cutting performance.
Metal Alloy Annealing and Degassing Bright annealing and hydrogen-free degassing of reactive and refractory metals such as titanium, zirconium, and nickel alloys. The high vacuum environment removes dissolved gases without surface oxidation. Produces bright, stress-relieved parts ready for subsequent processing or final use.
Quartz Glass Dehydroxylation Thermal treatment of fused quartz and silica glass to remove hydroxyl (OH⁻) groups, improving infrared and UV transmission. The vacuum accelerates outgassing at moderate temperatures, minimizing cristobalite formation. Enhances optical clarity and thermal stability for semiconductor, lighting, and fiber optic applications.
Precious Metal Brazing High-temperature brazing of jewelry, dental, and aerospace components using gold, silver, or nickel-based filler metals under vacuum or inert gas. Precise temperature control prevents overheating and ensures strong, void-free joints. Achieves hermetic, corrosion-resistant joints with minimal flux or post-processing.
R&D Material Synthesis Prototyping and small-batch synthesis of novel ceramic and metal matrix composites, catalyst materials, or solid-state electrolytes. The fully programmable controller allows testing of multiple heating profiles and atmospheres. Accelerates research by enabling rapid iteration and reproducible thermal processing.

Technical Specifications

Parameter Specification
Model TU-SJA
Power Supply Three-phase 380V, 50Hz
Heating Power 10 kW ±10% (single-phase 380V)
Design Temperature 1200°C
Rated Temperature Range 0–1200°C
Workspace Dimensions Φ60 × 60 mm (diameter × height)
Temperature Control Zones Single zone
Control Method Thermocouple with PID
Temperature Control Accuracy ±1°C
Cold Limit Vacuum 6.67 × 10⁻³ Pa (empty, cold, after bakeout)
Filling Gas Inert gas (e.g., argon, nitrogen)
Filling Pressure ≤0.05 MPa

Why Choose This Product

  • Proven Long-Term Reliability: Every unit is built with high-quality vacuum components, industrial-grade heaters, and robust structural welding. Extensive factory testing under actual process conditions ensures that the system meets specified vacuum and temperature performance, delivering dependable operation over years of continuous use in demanding laboratory environments.
  • Superior Build Quality and Precision: From the precision-machined hearth mechanism to the PID-tuned temperature control, attention to detail is evident throughout. The system maintains tight tolerances, resulting in excellent temperature uniformity and repeatable sintering outcomes, which are essential for valid experimentation and process scale-up.
  • Comprehensive After-Sales Support: Our global service network provides installation guidance, operator training, and ongoing technical support. We offer maintenance contracts and rapid spare parts delivery to minimize downtime, ensuring your research stays on schedule.
  • Flexible Customization Options: Recognizing that no two applications are identical, we offer custom workspace configurations, alternative heating elements, specialized gas handling, and software modifications. Our engineering team works closely with you to tailor the furnace to your specific material and throughput requirements.
  • Competitive Value for Investment: Combining advanced features typically found in larger floor-standing systems into a compact benchtop package, this furnace delivers exceptional price-performance. The integrated design reduces installation costs and complexity, providing a complete sintering solution without hidden extras. Contact us today to receive a detailed proposal and see how this system can enhance your laboratory capabilities.
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