Tube Furnace
Compact Split Tube Furnace with Integrated Vacuum System and Precision Temperature Calibrator
Item Number: TU-18
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Product Overview


This high-temperature processing system is a specialized thermal solution designed for precision-driven material science and industrial research. By combining a split-tube architecture with an integrated vacuum environment, the equipment allows for rapid sample loading and unloading without compromising the integrity of complex experimental setups. The system is engineered to facilitate uniform heating up to 1200°C, providing a stable platform for annealing, sintering, and chemical vapor deposition processes where atmospheric control is critical to the final material properties.
Targeted at advanced research laboratories and industrial R&D facilities, this unit provides the flexibility needed for multi-disciplinary studies. Whether used for semiconductor wafer processing or new battery chemistry development, the system offers a reliable and repeatable thermal environment. The inclusion of a dedicated temperature calibration assembly ensures that the user can verify real-time internal tube temperatures, bridging the gap between set-point parameters and actual sample exposure conditions.
Built for durability and long-term operational consistency, the equipment features a heavy-duty steel casing and high-purity alumina fibrous insulation. This combination not only ensures superior energy efficiency but also maintains a low external skin temperature during high-temp cycles. The robust engineering reflects a commitment to safety and precision, making it an essential asset for procurement teams seeking a reliable, high-performance thermal processing unit that meets the rigorous standards of modern material research and industrial heat treatment.
Key Features
- Precision Split-Tube Design: The lengthwise split-opening chamber allows for easy access to the process tube, facilitating the rapid insertion of samples or pre-assembled experimental rigs without requiring full disassembly of the vacuum flanges or gas lines.
- Advanced PID Temperature Control: This system utilizes a high-precision PID controller with 30 programmable segments, ensuring tight thermal accuracy of ±1°C and allowing for complex ramp and soak profiles tailored to specific material requirements.
- Integrated High-Vacuum System: Equipped with a 156 L/m double-step rotary vane vacuum pump and exhaust filtration, the unit can achieve vacuum levels as low as 1E-2 Torr, enabling contamination-free processing in controlled environments.
- Real-Time Temperature Calibration: An integrated NIST-standard OMEGA K-type thermocouple and digital calibrator allow operators to measure internal sample temperatures directly, providing a high level of confidence in experimental data and process repeatability.
- Superior Thermal Insulation: The chamber is lined with energy-efficient Al2O3 fibrous thermal insulation, which reduces heat loss and power consumption while ensuring rapid heating rates up to 10°C/min for increased laboratory throughput.
- Dual-Side Atmospheric Control: Featuring stainless steel vacuum flanges with a 1/4" barb gas inlet and KF25 gas outlet, the system supports both vacuum operation and flowing gas atmospheres for versatile chemical and physical vapor deposition processes.
- Mo-Doped High-Performance Heating Elements: The Fe-Cr-Al alloy heating elements, enhanced with Molybdenum doping, are designed for longevity and consistent performance at temperatures up to 1200°C, resisting oxidation and thermal fatigue.
- Modular Vacuum Flange Assembly: The heavy-duty SS flanges include integrated vacuum gauges and high-temperature seals, designed for quick assembly and reliable sealing during extended high-vacuum operations at elevated temperatures.
- Integrated Safety and Monitoring: The system includes internal safety blocks to prevent radiation heat loss and can be integrated with optional monitoring software for real-time data logging and remote recipe management via PC.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Semiconductor Annealing | Processing of silicon wafers and thin films in a vacuum or inert gas atmosphere to modify electrical properties. | Precise ±1°C control ensures uniform wafer characteristics. |
| Battery Material Synthesis | Calcination and sintering of cathode/anode powders under controlled pressure to optimize ionic conductivity. | Vacuum environment prevents oxidation of sensitive lithium compounds. |
| Carbon Nanotube Growth | Utilizing CVD processes to grow carbon nanostructures on various substrates within the quartz tube. | Split design allows for easy harvesting of delicate substrates. |
| Metallurgical Heat Treatment | Tempering and stress-relieving of metal alloys and small components in a contamination-free vacuum. | Internal calibrator ensures exact core temperature monitoring of samples. |
| Ceramic Sintering | High-temperature consolidation of ceramic powders into dense structural components. | Fibrous insulation supports stable ramps for crack-free ceramic production. |
| Catalyst Characterization | Testing the thermal stability and reactivity of chemical catalysts under specific flowing gas compositions. | Real-time monitoring via digital calibrator ensures accurate reaction data. |
| Aerospace Materials Testing | Subjecting advanced alloys to thermal cycles to simulate high-altitude or extreme thermal environments. | High heating rates allow for rapid thermal shock simulation. |
Technical Specifications
| Parameter | Specifications for TU-18 |
|---|---|
| Model Identifier | TU-18 |
| Casing Material | Heavy-duty steel with Al2O3 fibrous thermal insulation |
| Total Power | 1.75 KW |
| Input Voltage | AC 110V, Single Phase, 50/60 Hz (208V-240V available upon request) |
| Maximum Temperature | 1200 °C (< 1 hour) |
| Continuous Operating Temp | 1100 °C |
| Heating Rate | ≤ 10 °C/min |
| Standard Processing Tube | High-Purity Quartz: 50mm OD x 43mm ID x 600mm Length |
| Optional Processing Tube | 60mm OD Quartz with observation window available |
| Heating Zone Length | 200 mm (Single Zone) |
| Constant Temperature Zone | 100 mm (±2 °C @ 900 °C) |
| Temperature Controller | PID automatic control via PWM solid relay; 30-step programmable |
| Temperature Accuracy | ± 1 °C |
| Vacuum Flanges | Stainless Steel with 1/4" barb fitting, KF25 outlet, and TC feed-through |
| Vacuum Level | 1E-2 Torr (50 m-torr) with included mechanical pump |
| Vacuum Pump | Double Step Rotary Vane (156 L/m) with Exhaust Filter |
| Heating Elements | Fe-Cr-Al Alloy doped by Mo |
| Temperature Calibrator | OMEGA K-type thermocouple (18" x 1/4" Dia) with Digital Readout |
| Data Interface | USB and RS232 Interface for NIST-certified calibration data |
| Safety Blocks | Two fibrous ceramic tube blocks included to prevent radiation loss |
| Compliance | NRTL or CSA certification optional |
Why Choose This Furnace System
- Unmatched Measurement Precision: The integration of a dedicated, NIST-traceable temperature calibrator directly into the vacuum chamber allows for verification of sample temperatures that standard wall-mounted sensors cannot match.
- Engineered for Reliability: Utilizing industrial-grade Mo-doped heating elements and high-density alumina insulation, this system is built to withstand continuous use in demanding R&D environments without performance degradation.
- Complete Ready-to-Operate Package: Unlike systems that require separate procurement of vacuum components, this unit arrives with a high-capacity 156 L/m mechanical pump, all necessary flanges, and a quartz tube included.
- Flexible and Scalable Architecture: The split-tube design and modular flange system allow users to upgrade to larger tubes or turbomolecular pumps (achieving 10E-6 Torr) as research requirements evolve.
- Superior Build Quality: Every component, from the heavy-duty steel chassis to the precision PID electronics, is manufactured to meet the highest standards of industrial durability and user safety.
Please contact our technical sales team today for a formal quotation or to discuss a custom configuration tailored to your specific material processing requirements.
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