1100C High Temperature Vacuum Crucible Furnace with Quartz Chamber for Thermal Processing and Sintering

Tube Furnace

1100C High Temperature Vacuum Crucible Furnace with Quartz Chamber for Thermal Processing and Sintering

Item Number: TU-C05

Maximum Temperature: 1100°C Chamber Dimensions: 4.7" D x 8" H (120 mm x 200 mm) Vacuum Achievement: 10^-5 Torr (with Turbo Pump)
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Product Overview

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This high-performance vacuum crucible furnace represents a critical advancement in benchtop thermal processing technology, specifically engineered for material science laboratories and industrial R&D facilities. By combining a high-purity quartz chamber with robust vacuum capabilities, this system allows researchers to conduct sintering, annealing, and melting processes under strictly controlled atmospheric conditions. The core value proposition of this equipment lies in its ability to provide a clean, isolated environment that prevents oxidation and contamination, which is essential for developing next-generation ceramics, metals, and composite materials.

Primarily utilized in metallurgy, semiconductor research, and advanced ceramics manufacturing, the equipment serves as a versatile tool for both standard heat treatment and complex atmospheric synthesis. Its compact footprint masks a powerful heating array capable of reaching sustained high temperatures while maintaining exceptional thermal uniformity. The unit is particularly valued in academic settings for its transparency and ease of use, and in industrial settings for its consistent performance during repetitive testing cycles and small-batch production runs.

Engineered for longevity and reliability, this unit features a heavy-duty stainless steel casing and a specialized remote-operation controller box. These design choices ensure that the sensitive electronic components are protected from the radiant heat of the furnace body, while the anti-corrosive housing maintains its integrity in demanding laboratory environments. Procurement teams can invest with confidence, knowing the system is built to withstand the rigors of continuous thermal cycling without compromising on precision or safety.

Key Features

  • Precision-Engineered Quartz Chamber: The high-purity quartz tube offers excellent thermal shock resistance and chemical purity. Its transparent nature allows researchers to monitor sample changes during the heating process, providing invaluable visual data for sensitive R&D applications.
  • Dual-Controller Safety Architecture: The system utilizes a unique split-box design with two independent digital controllers. One primary unit manages the PID temperature curve, while a second dedicated monitor acts as an over-temperature watchdog, automatically cutting power to prevent equipment damage or process failure.
  • Superior Corrosion Resistance: Constructed with an SS316 stainless steel outer case, this furnace is designed to thrive in environments where corrosive gases or high humidity might degrade a standard powder-coated mild steel unit. This ensures a longer service life and professional aesthetic in industrial labs.
  • Advanced Vacuum Management: Equipped with high-integrity flanges and precision needle valves, the unit can achieve vacuum levels down to 10^-5 Torr when paired with a turbo pump. The inclusion of KF16 and KF25 ports allows for seamless integration with industrial-standard vacuum gauges and pumps.
  • Programmable Thermal Profiles: The primary PID controller supports 30 programmable segments, allowing for complex ramp, soak, and cool-down sequences. This precision control is vital for achieving the exact microstructure properties required in modern material science.
  • Remote Operation Interface: By separating the temperature controller from the main heating chamber, the system protects electronic components from thermal stress and allows operators to manage the furnace from a safe distance or a centralized control panel through the integrated RS485 port.
  • High-Efficiency Insulation: The heating chamber utilizes premium ceramic fiber insulation, which minimizes heat loss to the external environment, reduces energy consumption, and ensures the outer casing remains safe to touch during extended operation.
  • Integrated Gas Control: Featuring a 1/4" gas inlet and industrial-grade needle valves, the system allows for the precise introduction of inert gases, enabling researchers to transition from vacuum to atmospheric processing without breaking the chamber seal.

Applications

Application Description Key Benefit
Solid State Sintering High-temperature consolidation of ceramic or metal powders under vacuum to minimize porosity. Enhanced mechanical strength and density in final materials.
Thin Film Annealing Post-deposition heat treatment of thin films on quartz or silicon substrates to improve crystal structure. Improved electrical conductivity and structural uniformity.
Precious Metal Melting Controlled melting of gold, silver, or platinum alloys in a contamination-free quartz environment. Superior purity and reduction of oxidative waste loss.
Catalyst Synthesis Thermal activation of catalytic materials under specific inert or reduced atmospheric pressures. Optimized surface area and catalytic reactivity for industrial use.
Glass Research Study of transition temperatures and phase changes in specialized optical or glass-ceramic materials. High visual accessibility for observing phase transformation.
Powder Metallurgy Sintering of refractory metal powders that require strictly oxygen-free environments to prevent brittleness. Prevention of oxidation and consistent metallurgical properties.
Semiconductor R&D Diffusion and oxidation studies for silicon-based devices in a high-purity thermal environment. Minimized metallic contamination for high-yield research outcomes.

Technical Specifications

Attribute Detailed Specification of TU-C05
Model Identifier TU-C05
Input Voltage AC 110V, Single Phase, 50/60Hz (220V available on request)
Power Consumption 1.5 KW Maximum
Rated Current/Fuse 20A
Max. Operating Temperature 1100°C (Short term < 1 hour)
Continuous Working Temp. < 1000°C
Maximum Heating Rate 20°C per minute
Chamber Construction SS316 Stainless Steel for anti-corrosive processing
Heating Chamber Dimensions 4.7" Diameter x 8" Height (120 mm ID x 200 mm H)
Quartz Tube Dimensions 100 mm OD x 94 mm ID x 250 mm L
Vacuum Flange Configuration One flange with 1/4" gas inlet, needle valve, KF16 port, and KF25 port
Included Vacuum Hardware KF25 Vacuum Right-Angle Valve and mounting hardware
Vacuum Capability 10^-2 Torr (Mechanical Pump) / 10^-5 Torr (Turbo Pump)
Temperature Accuracy ±1.0°C
Thermocouple Type Two Omega K-type thermocouples included
Control Methodology PID automatic control with auto-tune and 30-segment programming
Safety Features Over-heat protection and thermal couple break protection
Data Communication RS485 Port installed for PC operation
Certification CE Certified (NRTL Certification available upon request)

Why Choose Us

  • Industrial Grade Reliability: Built with SS316 stainless steel and high-purity quartz, this system is designed for long-term operational consistency in high-throughput research environments, far outperforming entry-level lab ovens.
  • Safety-Centric Engineering: The dual-controller architecture and remote-station design prioritize operator safety and equipment protection, reducing the risk of catastrophic failures during overnight or long-duration processes.
  • Precision Control for Research: With 30-segment PID programming and ±1°C accuracy, researchers can replicate complex thermal cycles with industrial-grade precision, ensuring publishable and repeatable experimental data.
  • Customizable Atmosphere Support: Whether your process requires high vacuum or inert gas purging, the versatile port configuration—including KF16 and KF25 standards—makes this system compatible with a wide array of laboratory equipment.
  • Comprehensive Compliance: CE certification comes standard, with optional NRTL certification to meet the specific safety mandates of your facility or institution, providing peace of mind for procurement and safety officers alike.

Our engineering team is ready to assist you in configuring the ideal vacuum and gas delivery setup for your specific research needs. Contact us today for a detailed quote or to discuss custom modifications for your unique thermal processing applications.

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