Vacuum Melt Spinning Integrated Furnace for Ribbon and Wire

Vacuum Melt-Spinning Furnace

Vacuum Melt Spinning Integrated Furnace for Ribbon and Wire

Item Number: TU-SDE

Ultimate Vacuum: 6.7×10⁻⁴ Pa (selectable) Maximum Temperature: ≥1700°C Ribbon Spinning Capacity: 100–500 g
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Product Overview

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This vacuum melt spinning integrated furnace merges induction melting, ribbon casting, and wire drawing in a single vacuum enclosure, offering researchers a complete platform for rapid solidification of metastable materials. Designed specifically for synthesizing amorphous, nanocrystalline, and bulk metallic glass alloys, the system enables precise control over quenching rates and atmospheric purity—critical for reproducible material properties.

Frequently employed in advanced magnetics research, the unit facilitates the production of thin ribbons for low-loss transformer cores, flakes for high-performance permanent magnets, and fine wires for magnetic sensors. Beyond magnetics, it supports development of high-entropy alloys, shape memory materials, and catalytic bulk metallic glasses. Its versatility makes it an indispensable tool in both academic laboratories and industrial R&D centers.

Engineered with a fully stainless steel body and equipped with comprehensive safety interlocks, this furnace is built for continuous operation. The modular design simplifies maintenance and allows future upgrades, while the reliable IGBT power supply and high-precision vacuum system ensure that process parameters remain stable over thousands of cycles, giving researchers the confidence to push the boundaries of materials science.

Key Features

  • Integrated Melt Spinning Functions: This system streamlines the entire process from alloy melting to thin ribbon or wire fabrication, all within one vacuum chamber. The ribbon spinning roller (Φ300×100 mm) handles charges up to 500 g, producing foils 20–100 µm thick, while the wire spinning roller (Φ200×10 mm) processes 50–150 g into continuous wires as fine as 60 µm. Quick-change tooling enables rapid transition between modes.
  • All Stainless Steel Construction: The vacuum chamber, door, and frame are manufactured from medical-grade stainless steel, providing exceptional corrosion resistance and enabling straightforward cleaning. This ensures no rust or contamination, even when processing reactive alloys or after repeated harsh solvent cleaning.
  • Ultra-High-Temperature Capability with IGBT Power: A high-frequency IGBT induction heater delivers clean, controllable power, allowing melt temperatures surpassing 1700°C. The precise energy control facilitates melting of refractory metals and complex alloys without overheating, thereby preserving material composition.
  • Selectable Vacuum Performance: The two-stage vacuum system, consisting of a rotary vane pump and either a diffusion or turbomolecular pump (based on configuration), offers a choice of base pressures: 10 Pa, 5×10⁻³ Pa, or 6.7×10⁻⁴ Pa. This flexibility lets users balance cost and purification needs, from inert gas partial pressure to high-vacuum outgassing.
  • Intuitive Touchscreen Automation: The PLC-based control panel with a 7-inch color touchscreen displays real-time temperature, vacuum, and rotation speed. Password-protected access levels (operator, engineer, administrator) secure critical parameters and facilitate compliance with data integrity requirements in regulated R&D settings.
  • Ergonomic Side-Opening Chamber: Unlike top-loading designs, the side-hinged door offers full, unimpeded access to both the crucible and the spinning rollers, simplifying loading of irregularly shaped feedstock and routine cleaning. This design reduces physical strain and speeds up turnaround.
  • Large Observation Window for Process Monitoring: A robust viewport, positioned for an optimum angle, allows continuous visual monitoring of the melt pool surface and ejection stream. This real-time feedback is invaluable for assessing melt viscosity, jet stability, and optimal quenching distance.
  • Extreme Quenching Rates: The water-cooled copper rollers spin at high circumferential speeds, generating cooling rates on the order of 10⁵–10⁶ K/s. This rapid solidification is essential for freezing the amorphous structure and achieving the desired physical properties in melt-spun products.
  • Comprehensive Safety System: Integrated hardware trips for vacuum loss, overtemperature, cooling water failure, and door interlock guarantee safe operation. The PLC software further enforces a startup sequence that cannot be bypassed, protecting both personnel and the equipment.
  • Versatile Crucible Configurations: A range of crucible materials (alumina, magnesia, zirconia, graphite) and sizes accommodate diverse alloy types—from reactive titanium to noble metal-based glasses—ensuring compatibility with your entire research portfolio.

Applications

Application Description Key Benefit
Amorphous Soft Magnetic Ribbons Continuous casting of Fe-Si-B and Fe-Co-based alloys into ultra-thin ribbons (20–50 µm) at high speeds. These ribbons are wound into toroidal cores for low-loss power transformers and high-frequency inductors in renewable energy systems. Significantly reduced core loss and CO₂ emissions over silicon steel.
Rare-Earth Permanent Magnet Flakes Melt spinning of Nd-Fe-B and Sm-Co alloys to produce nanocrystalline flakes with fine grain structure (<100 nm). These flakes are essential raw material for bonded magnets used in electric vehicle traction motors and wind turbine generators. High coercivity without heavy rare-earth additions, lowering cost and supply risk.
Amorphous Wires for GMI Sensors Direct jet casting of Co-rich amorphous wires with diameters as small as 60 µm. Their giant magneto-impedance effect enables highly sensitive magnetic field sensing for applications in automotive ABS, non-destructive testing, and biomedical diagnostics. Ultra-high sensitivity, compact form factor, and low power consumption.
Bulk Metallic Glass Precursors Rapid quenching of Zr-, Ti-, or Pd-based bulk glass-formers into ribbons for thermal analysis (DSC) and secondary processing. Enables determination of critical casting thickness and crystallization kinetics before scaling up to bulk parts. Accelerates alloy development and reduces costly trial-and-error in casting.
Nanocrystalline Soft Magnetic Cores Production of Finemet-type (Fe-Cu-Nb-Si-B) ribbons that, after optimized annealing, yield a nanocrystalline structure with extremely high permeability (μᵢ > 100,000) and near-zero magnetostriction, used in precision current transformers and EMC filters. Best-in-class magnetic softness and low audible noise.
High-Entropy Alloy R&D Solidify equiatomic or near-equiatomic multi-component alloys at extreme rates to suppress intermetallic formation. The resulting ribbons are ideal for screening mechanical properties, phase stability, and catalytic activity. Expands the compositional landscape for next-generation structural and functional alloys.
Magnetic Shape Memory Ribbons Cast Ni-Mn-Ga Heusler alloys into ribbons that exhibit a magnetic-field-induced strain through twin boundary motion. Rapid solidification preserves the necessary chemical order and refines grain size, enhancing actuator performance. Larger reversible strain without mechanical fatigue.
Catalytic Metallic Glass Precursors Fabricate amorphous ribbons (Fe-, Al-, or Mg-based) that serve as precursors for nanoporous catalysts via dealloying. High cooling rates ensure chemical homogeneity, critical for uniform porosity and high catalytic efficiency in hydrogen evolution and oxygen reduction. High specific surface area and sustainable catalytic activity.

Technical Specifications

Parameter Specification
Model TU-SDE
Total Power 25 kW
Power Supply 3-phase, 380 V, 50 Hz
Ultimate Vacuum Selectable: 10 Pa, 5×10⁻³ Pa, 6.7×10⁻⁴ Pa
Vacuum Pumping Configuration Two-stage (rotary vane pump + diffusion or turbomolecular pump)
Ribbon Spinning Copper Roller Φ300 mm × 100 mm
Ribbon Capacity 100–500 g (depending on alloy density)
Wire Spinning Roller Φ200 mm × 10 mm
Wire Capacity 50–150 g (depending on alloy density)
Control System PLC with color touchscreen HMI, password-protected user levels
Maximum Melt Temperature ≥1700°C
Heating Method IGBT high-frequency induction
Chamber Construction Full stainless steel body, vertical side-opening door
Observation Window Large-diameter high-strength glass viewport

Additional customizations, including different roller diameters, specialized crucible materials, and advanced vacuum capabilities, are available upon request.

Why Choose This Product

  • Decades of Domain Expertise: We bring a deep understanding of rapid solidification technology, evolving our designs based on feedback from leading materials science institutes. This furnace embodies robust vacuum engineering, precision motion control, and reliable electrical systems that deliver consistent amorphous yield run after run.
  • Custom-Engineered Solutions: Off-the-shelf rarely fits cutting-edge research. We work alongside your team to modify roller dimensions, add gas quenching nozzles, integrate a sample transfer interlock, or adapt the control software to match your experimental matrix—turning a standard platform into a unique instrument.
  • Operational Safety and Regulatory Compliance: Designed to meet international safety standards, the system features redundant safety interlocks for vacuum, power, and cooling. The touchscreen’s permission-based access prevents unintended process changes, an essential feature for multi-user labs and ISO-certified facilities.
  • Built for a Lifetime of Service: From the stainless steel chamber to the heavy-duty vacuum pumps and solid-state electronics, every component is chosen for durability. Customers report over a decade of reliable operation with minimal downtime, a testament to our manufacturing quality.
  • Global Support and Peace of Mind: Our service doesn’t end at shipment. We offer installation, on-site training, application support, and a comprehensive warranty. A worldwide network of service engineers ensures that help is never far away, keeping your research on track.

Contact us now to discuss your specific requirements, and let us provide a competitive quotation for a personalized vacuum melt spinning solution.

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