1200C Hydrogen Atmosphere Box Furnace with 5 Heated Sides and 64L Chamber

Atmosphere Furnace

1200C Hydrogen Atmosphere Box Furnace with 5 Heated Sides and 64L Chamber

Item Number: TU-QF27

Maximum Temperature: 1200°C Chamber Capacity: 64 Liters (400x400x400mm) Heating Configuration: 5-Sided for ±1°C Uniformity
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Product Overview

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This high-performance thermal processing system is a specialized box furnace engineered for material synthesis and heat treatment within a controlled hydrogen environment. Capable of reaching temperatures up to 1200ºC, the equipment provides a robust solution for researchers and industrial engineers working with complex reduction reactions. By integrating a vacuum-sealed stainless steel case with an advanced water-cooling jacket, the unit ensures stable operation under positive pressure while protecting the structural integrity of the furnace during high-temperature cycles.

The primary use cases for this system involve the preparation of advanced materials that require a strictly reduced atmosphere, such as phosphorus compounds and titanium alloys. Beyond hydrogen-rich processes, the equipment is versatile enough to handle heat treatments under inert gases, oxygen, or non-flammable mixed gases. This flexibility makes it a cornerstone tool for laboratories focusing on metallurgy, semiconductor development, and catalyst research where atmospheric purity and thermal precision are non-negotiable requirements.

Reliability is at the core of this unit's design. Featuring industrial-grade Kanthal Fe-Cr-Al alloy heating elements and a multi-sided heating configuration, it delivers exceptional temperature uniformity across the entire 64-liter chamber. High-purity fibrous alumina insulation and a reflective Al2O3 coating maximize energy efficiency, ensuring that the system maintains consistent performance even under the most demanding R&D schedules. The inclusion of a dedicated H2 burning system and automatic safety shut-off valves provides the operational confidence necessary for handling flammable gases in a professional laboratory setting.

Key Features

  • Superior Five-Sided Heating Configuration: Unlike standard furnaces that only heat from two or three directions, this system utilizes heating elements on the left, right, bottom, back, and front. This comprehensive coverage ensures the most uniform temperature distribution possible throughout the heating chamber, which is critical for consistent material properties in batch processing.
  • Advanced Hydrogen Safety Integration: The equipment is equipped with a built-in hydrogen burning control system. An integrated ignition device incinerates flowing gas and monitors burner temperature; if the system detects a flame failure, the H2 delivery valve is automatically shut down to prevent gas accumulation and ensure facility safety.
  • High-Performance Vacuum and Pressure Management: The double-layer stainless steel structure is designed for maximum vacuum integrity and safety, capable of maintaining a positive pressure up to 0.06 MPa and a vacuum down to -0.09 MPa. This allows for rigorous purging protocols and precise control over the internal environment.
  • Premium Thermal Insulation: The chamber is lined with energy-saving 1500-grade fibrous alumina insulation and coated with a high-purity reflective Al2O3 layer. This engineering choice reduces heat loss to the external environment, accelerates ramp rates, and significantly lowers operational energy costs.
  • Precision PID Temperature Regulation: Utilizing a sophisticated PID controller with 30 programmable segments, the furnace allows for complex ramping, cooling, and dwelling steps. The system maintains a temperature accuracy of ±1°C, providing the repeatable thermal profiles essential for scientific validation.
  • Industrial-Grade Kanthal Heating Elements: The unit employs 1300°C grade Kanthal Fe-Cr-Al resistance wires, known for their exceptional oxidation resistance and long-term stability under high-temperature cycling, ensuring minimal downtime for element replacement.
  • Integrated Cooling Infrastructure: A heavy-duty water-cooling jacket protects the front door and sealing flanges, while an air-cooled outer shell keeps the exterior surface temperatures safe for operators. A built-in 16L/min recirculating water chiller is included to maintain the integrity of the vacuum seals.
  • Comprehensive Gas Flow Control: Two independent large flow meters (for N2 and H2) are mounted on the front panel, allowing operators to transition seamlessly from inert gas purging to active hydrogen introduction with high volumetric precision.

Applications

Application Description Key Benefit
Titanium Alloy Synthesis Processing Ti-based alloys in a reduced atmosphere to prevent oxidation and nitrogen contamination. Superior structural integrity and purity of treated alloys.
Catalyst Activation Mechanochemical and thermal activation of catalysts for CO2 reduction and green energy applications. Precise control over reduction states and surface morphology.
Phosphorus Production Synthesis of refined phosphorus materials requiring high-temperature reduction in safe H2 environments. Minimized risk of explosion with integrated H2 burning sensors.
Powder Metallurgy Sintering of metallic powders under inert or reducing gases to achieve high density. High temperature uniformity avoids localized structural weaknesses.
CVD/PECVD Support Serving as the thermal base for chemical vapor deposition processes using various precursor gases. Adaptable gas handling and vacuum seal capabilities for custom R&D.
Annealing of Semiconductors Precision heat treatment of wafer components in a non-oxidizing atmosphere. ±1°C accuracy prevents thermal stress and doping fluctuations.
Ceramic Co-firing High-temperature processing of advanced ceramics under controlled atmospheric conditions. 64L capacity allows for significant batch sizes with uniform results.

Technical Specifications

Parameter Specification Details for TU-QF27
Item Number TU-QF27
Chamber Dimensions 400mm x 400mm x 400mm (~16" x 16" x 16")
Total Volume 64 Liters
Heating Method 5-sided heating (Left, Right, Bottom, Back, Front)
Heating Elements 1300°C Grade Kanthal Fe-Cr-Al resistance wire
Maximum Temperature 1200°C
Heating Rate Recommended: ≤ 10°C/min; Max: 20°C/min
Temperature Accuracy ± 1°C
Uniform Zone (Center 250mm) ± 1°C (cubic zone)
Uniform Zone (Center 300mm) ± 5°C (cubic zone)
Max Sample Loading 35 kg
Vacuum Integrity Up to -0.09 Mpa
Positive Pressure Cap Up to 0.06 Mpa
Flow Meter Ranges N2: 0–3.5 L/min; H2: 0–3.5 L/min
Cooling System 16 L/min recirculating water chiller for seals; Air-cooled shell
Power Supply 10 KW; 208-240V 3-Phase, 50/60Hz (380V-460V optional)
Controller FA-YD518P-AG PID with 30 segments and auto-tune
Communication Default DB9 PC port; LabVIEW/Eurotherm options available
Compliance CE Certified; MET Certified (Controller)

Why Choose This Furnace

  • Unmatched Thermal Uniformity: The 5-sided heating design is specifically engineered for critical processes where even a few degrees of variance can compromise material characteristics. This system provides a 250mm cubic zone of ±1°C precision.
  • Safety-First Engineering: Hydrogen processing carries inherent risks. This unit manages those risks via integrated flame sensors, auto-shutoff valves, and a double-walled water-cooled jacket designed to handle positive pressure safely.
  • Robust Commercial Build: Designed for the rigors of industrial R&D, the use of Kanthal elements and 1500-grade insulation ensures that this furnace is a long-term investment with low maintenance requirements.
  • High-Capacity Processing: The 64-liter chamber and 35kg loading capacity allow for larger sample sizes or batch synthesis, bridging the gap between small-scale lab experiments and pilot-scale production.
  • Energy Efficiency: Reflective Al2O3 coatings and high-density fibrous insulation minimize heat radiation to the lab environment, reducing utility costs and improving operator comfort.

Our technical team is ready to discuss your specific atmospheric requirements or help you configure a custom solution for your facility. Contact us today for a technical consultation or a formal quotation.

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