Tube Furnace
High Temperature Vertical Three Zone Powder Spheroidizing Furnace for Advanced Material Synthesis and Industrial Thermal Processing
Item Number: TU-C21
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Product Overview




This high-temperature vertical processing system offers a precision-engineered solution for material scientists and industrial researchers focused on powder spheroidizing and morphology optimization. By integrating a three-zone furnace with a speed-adjustable vibration feeder and an efficient water-cooled collection mechanism, the equipment enables the continuous processing of fine powders under controlled atmospheric or vacuum conditions. It is specifically designed to meet the rigorous demands of modern material synthesis, where particle shape consistency is paramount for the performance of high-tech materials.
Primarily utilized in the development of advanced magnetic materials, metal powders for additive manufacturing, and high-purity ceramics, this unit provides a versatile platform for thermal processing up to 1700°C. The vertical orientation utilizes gravity as a dynamic force, allowing powders to pass through precisely controlled thermal gradients during descent. This flight path is critical for achieving uniform spheroidization through surface tension-driven reshaping, making this system a cornerstone for R&D labs and industrial pilot lines seeking professional-grade results.
Built with industrial-grade components and a heavy-duty double-shell frame, the equipment ensures long-term reliability and repeatable performance under demanding conditions. The air-cooling system protects internal components and maintains a safe exterior temperature even during prolonged high-heat cycles. Users can rely on this robust thermal system for critical processes where temperature stability and mechanical durability are essential for operational success in material science and industrial metallurgy.
Key Features
- Independent Triple-Zone Thermal Control: The heating chamber is divided into three separate segments, each 400mm in length, allowing operators to create specific temperature gradients or a long, uniform isothermal zone to accommodate complex powder processing requirements.
- Precision Vibration Feeding Mechanism: Featuring a 5L stainless steel storage chamber, the speed-adjustable feeder ensures a constant and non-clumping flow of powder materials into the furnace tube at rates between 20ml and 90ml per minute.
- Rapid Water-Cooled Quenching System: A specialized collection tank at the base of the vertical tube enables immediate thermal arrest, preserving the spherical morphology of the particles developed during the high-temperature flight phase.
- Advanced 30-Segment PID Regulation: The control system utilizes sophisticated proportional-integral-derivative algorithms with 30 programmable segments for precise ramping, dwelling, and cooling cycles, maintaining thermal accuracy within ±1°C.
- High-Performance Atmosphere and Vacuum Versatility: Equipped with KF25 vacuum flanges and a sealed chamber design, the system supports sintering in inert atmospheres or under high vacuum (up to 10-4 Torr with optional molecular pumps) to prevent oxidation of sensitive materials.
- Industrial-Grade Type B Thermocouples: High-purity Type B sensors provide accurate feedback for high-temperature operations, ensuring that the continuous working temperature of 1600°C is monitored with the highest levels of stability and sensitivity.
- Enhanced Safety and Cooling Architecture: The double-shell structure includes an integrated fan-assisted air cooling system that reduces the exterior casing temperature, while built-in over-temperature and thermocouple failure alarms protect the hardware and the environment.
- Scalable Digital Communication: The unit is equipped with a standard DB9 PC communication port, allowing for optional Labview-based software integration for recipe management, data logging, and remote monitoring via a desktop or laptop interface.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Additive Manufacturing | Spheroidizing irregular metal powders for use in SLM, EBM, and other 3D printing technologies. | Enhanced powder flowability and higher packing density for superior part quality. |
| Magnetic Materials | Heat treatment and conditioning of rare-earth and magnetic alloy powders. | Improved magnetic properties through controlled recrystallization and morphology. |
| Battery Research | Processing of cathode and anode precursors to optimize particle size and shape. | Increased specific surface area control and better electrolyte interaction. |
| Aerospace Coatings | Production of uniform spherical ceramic and alloy powders for thermal spray and bond coat applications. | More consistent coating thickness and reduced nozzle wear during spraying processes. |
| Catalyst Synthesis | Preparation of spherical support materials for chemical and petrochemical industry reactors. | Reduced pressure drop in fixed-bed reactors and improved surface reactivity. |
| Refractory Materials | High-temperature fusion and shaping of advanced refractory grains for industrial insulation. | Superior thermal shock resistance and mechanical durability of the final product. |
| Solid Oxide Fuel Cells | Synthesis of specialized ceramic powders for SOFC electrolytes and electrodes. | Optimized microstructure for enhanced ionic conductivity and structural integrity. |
| High-Purity Metallurgy | Spheroidizing and cleaning of high-purity metal particles for specialized metallurgical research. | Removal of volatile impurities and achievement of high-density crystalline structures. |
Technical Specifications
| Parameter Group | Specification Detail | Value / Measurement |
|---|---|---|
| Model Identification | Product Item Number | TU-C21 |
| Power Management | Power Supply | Three-phase AC 380V, 50/60Hz |
| Maximum Power | 30KW Max | |
| Circuit Protection | 63A Air Circuit Breaker Required | |
| Temperature Performance | Maximum Temperature | 1700°C |
| Continuous Working Temp | 1600°C | |
| Temperature Control Accuracy | ±1°C | |
| Thermocouple Type | Type B | |
| Heating Rate (≤1400°C) | ≤ 10°C / min | |
| Heating Rate (1400-1600°C) | ≤ 5°C / min | |
| Heating Configuration | Heating Zones | Three Zones (400mm + 400mm + 400mm) |
| Total Thermal Zone Length | 1200mm | |
| Tube Size | φ 60 mm x 1800 mm | |
| Feeding System | Chamber Volume | 5L (Stainless Steel) |
| Feeding Rate | 20ml to 90ml / min | |
| Feed Sample Capacity | Diameter ≤ 5mm | |
| Vacuum & Collection | Vacuum Level (Mechanical) | $10^{-2}$ Torr |
| Vacuum Level (Molecular) | $10^{-4}$ Torr | |
| Vacuum Interface | KF25 | |
| Collection Tank | Water-cooled with 30mm observation window | |
| Controller Interface | Programming | 30-segment programmable PID |
| Safety Alarms | Over-temperature and Thermocouple failure | |
| Connectivity | DB9 Communication Port | |
| Compliance | Standard Certifications | CE Certified; NRTL (UL61010) or CSA available |
Why Choose This Spheroidizing System
Choosing this vertical thermal system represents a significant upgrade in processing capability for any organization involved in advanced powder metallurgy. The unique combination of a high-temperature triple-zone design and an integrated vibration feeder allows for a level of process control that horizontal furnaces simply cannot match. By optimizing the descent profile of the powder through distinct thermal stages, researchers can achieve near-perfect spherical morphology, which is essential for the flowability and performance of advanced material additives.
Engineering excellence is evident in every component of this unit. From the precise Type B thermocouples that ensure accurate high-heat management to the water-cooled collection tank that prevents particle agglomeration upon exit, the system is designed for high-yield, high-quality production. The robust mechanical construction and the use of premium heating elements ensure that this equipment remains operational even under the most strenuous industrial cycles, providing a reliable platform for year-round research and production tasks.
Beyond raw performance, safety and certification are at the core of this furnace's design. The CE-certified architecture and the availability of NRTL or CSA compliance mean that this system can be integrated into world-class laboratories with no compromises on local safety standards. The ability to customize the atmospheric environment—ranging from protective gas flows to high-vacuum levels—further ensures that this furnace can grow alongside your research needs, accommodating everything from simple oxides to oxygen-sensitive rare-earth alloys.
This system is more than just a furnace; it is a complete powder processing solution designed for longevity, precision, and efficiency. Whether you are scaling a pilot line or conducting foundational research in material science, this equipment delivers the consistency and reliability required for groundbreaking discoveries.
Contact our technical sales team today to request a quote or to discuss a customized configuration tailored specifically to your laboratory's powder processing requirements.
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