Three Temperature Zone Rotating Tube Furnace for Material Sintering and Controlled Atmospheric Heat Treatment

Tube Furnace

Three Temperature Zone Rotating Tube Furnace for Material Sintering and Controlled Atmospheric Heat Treatment

Item Number: TU-GS12

Maximum Temperature: 1200 ℃ Rotation Speed: 1 - 20 RPM Control Precision: +/- 1 ℃
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Product Overview

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This system is a high-performance rotating tube furnace specifically engineered for continuous thermal processing of materials requiring simultaneous heat and agitation. By integrating a three-zone heating configuration with a mechanical rotation and inclination mechanism, the equipment ensures that powders and granular materials are exposed to a perfectly uniform temperature field. This design is critical for achieving consistent phase transformations, chemical vapor deposition, and homogenous sintering results that static furnaces cannot provide. The robust mechanical build combined with high-precision electronics makes this unit a cornerstone for material science laboratories and industrial pilot production lines.

Primary use cases for this equipment include the synthesis of battery materials, catalyst preparation, and the calcination of advanced ceramics. Its ability to operate under vacuum or specific gas atmospheres allows researchers to replicate complex industrial environments at a laboratory scale. Targeted industries include lithium-ion battery manufacturing, metallurgy, chemical engineering, and semiconductor development. The system’s flexibility in handling different tube diameters and atmosphere requirements ensures it can adapt to evolving research needs without sacrificing performance or precision.

Built for demanding industrial R&D, this unit prioritizes reliability through the use of premium components such as Swedish-made heating elements and advanced Japanese-engineered insulation. The dual-layered housing design keeps the external surface temperature safe while the internal PID controllers maintain strict thermal stability. This dedication to build quality ensures consistent operation during long-cycle experiments, providing procurement teams and lead researchers with the confidence that their critical data and material outputs are protected by industrial-grade engineering standards.

Key Features

  • Triple-Zone Temperature Control: The heating chamber is divided into three independently controlled zones, allowing for the creation of precise thermal gradients or a massive uniform isothermal zone to accommodate complex multi-step chemical reactions.
  • Premium Swedish Kanthal A1 Elements: Equipped with imported resistance wire capable of reaching 1420℃ surface temperatures, these elements are integrated to prevent slag fallout and oxidation, ensuring a clean processing environment and a long service life of up to two years under standard operation.
  • High-Purity Alumina Polycrystalline Insulation: Utilizing advanced Japanese vacuum suction and filter molding technology, the chamber fiber is high-density and high-purity, offering superior thermal retention and energy efficiency compared to traditional refractory materials.
  • Dynamic Rotation and Inclination: The system features an infinitely variable speed motor (1-20 RPM) and an adjustable tilt range (0-40°), allowing for the controlled movement of materials through the tube to ensure internal and external material consistency.
  • Sophisticated Thermal Engineering: The spacing and pitch of the heating elements are optimized through thermal software simulation to eliminate cold spots, providing a highly balanced temperature field across the entire tube length.
  • Integrated Safety Protection: To protect operators and the equipment, the unit includes an automatic power-cut system that activates if the chamber cover is opened, alongside over-temperature and thermocouple failure protections.
  • Computer Communication Interface: Standard RS485 connectivity and dedicated software allow for real-time remote monitoring, data logging of PV and SV values, and the ability to draw and store temperature curves for audit-ready documentation.
  • Advanced PID Tuning: The 30-segment intelligent program controller features self-tuning capabilities and power-failure memory, ensuring that processes resume seamlessly from the point of interruption without restarting the entire cycle.
  • Industrial Grade Components: Featuring SEMIKRON silicon control and Chint electrical components, the internal circuitry is designed for high-current durability and minimal electromagnetic interference.

Applications

Application Description Key Benefit
Lithium Battery Cathode Production Controlled calcination of cathode powders in a rotating environment to prevent agglomeration. Superior crystalline structure and electrochemical performance consistency.
Catalyst Synthesis High-temperature gas-solid reactions for the production of petrochemical and environmental catalysts. High surface area and uniform active site distribution through constant rotation.
Carbon Nanotube Growth Utilizing CVD processes within a controlled gas flow to grow nanotubes on substrates or powders. High throughput and precise control over temperature gradients for specific diameters.
Graphene Research Thermal exfoliation or vapor deposition on powder substrates under high vacuum. Repeatable material quality and high-purity output due to vacuum-tight sealing.
Powder Metallurgy Sintering of metal powders and alloys to achieve specific density and grain size. Prevents local overheating and ensures internal material homogeneity.
Pharmaceutical Processing Controlled heat treatment of specialized chemical compounds and drug precursors. Precise atmospheric control prevents contamination and ensures molecular stability.
Ceramic Calcination Processing of technical ceramics and advanced oxide materials at high temperatures. Reduced processing time and elimination of thermal stress within the material bulk.
Rare Earth Extraction High-temperature purification and separation processes for rare earth elements. Exceptional resistance to high-temperature oxidation and chemical erosion.

Technical Specifications

Parameter Specification (TU-GS12-I) Specification (TU-GS12-II)
Model Identifier TU-GS12-I TU-GS12-II
Maximum Temperature 1200 ℃ 1200 ℃
Rated Temperature 1100 ℃ 1100 ℃
Tube Dimensions (OD x L) Dia 60 × 1400 mm Dia 120 × 1400 mm
Heating Elements Swedish Kanthal A1 Resistance Wire Swedish Kanthal A1 Resistance Wire
Power Output 4.5 KW 6 KW
Supply Voltage 220V, Single Phase 220V, Single Phase
Rotation Speed 1 - 20 RPM (Infinitely Variable) 1 - 20 RPM (Infinitely Variable)
Inclination Angle Range 0 ~ 40° 0 ~ 40°
Control Precision +/- 1 ℃ +/- 1 ℃
Chamber Material Alumina Polycrystalline Fiber Alumina Polycrystalline Fiber
Program Controller 30-Segment Intelligent PID 30-Segment Intelligent PID
Heating Rate ≤ 30 ℃/Min (15 ℃/Min recommended) ≤ 30 ℃/Min (15 ℃/Min recommended)
Thermocouple Type K Type K Type
Trigger Phase-shifted Trigger Phase-shifted Trigger
Overall Dimensions 800 × 370 × 1050 mm 800 × 440 × 1100 mm
Surface Temperature ≤ 45 ℃ ≤ 45 ℃
Motor & Lift Power 40W (Rotation) / 40W (Lifting) 40W (Rotation) / 40W (Lifting)
Vacuum Capabilities Optional: 10Pa, 0.1Pa, or 10^-3 Pa Optional: 10Pa, 0.1Pa, or 10^-3 Pa

Why Choose Three Temperature Zone Rotating Tube Furnace

  • Proven Thermal Homogeneity: The combination of three-zone heating and variable speed rotation ensures that every particle of your material experiences the exact same thermal profile, eliminating the inconsistencies found in static tube furnaces.
  • Premium Material Construction: By utilizing Swedish Kanthal A1 elements and Japanese-inspired chamber molding, this furnace offers a significantly longer operational lifespan and higher resistance to thermal cycling fatigue.
  • Flexible Process Control: Whether you require high vacuum, specialized gas atmospheres via mass flow meters, or precise temperature gradients, this modular system can be customized to meet specific R&D requirements.
  • Data Integrity and Connectivity: With standard 485 communication and real-time data logging, your research data is preserved with high resolution, ensuring compliance with industrial quality standards and research protocols.
  • Unmatched Safety Engineering: From the open-cover protection to the leakage protectors and over-temperature alarms, this equipment is built to safeguard your facility, your personnel, and your samples.

Contact us today to discuss your specific thermal processing requirements or to receive a tailored quotation for your laboratory. Our engineering team is ready to assist you with custom configurations and specialized atmosphere solutions.

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