1200°C Bottom Loading Vacuum Furnace with Rapid Gas Cooling and 8.6 Inch Diameter Quartz Chamber

Muffle Furnace

1200°C Bottom Loading Vacuum Furnace with Rapid Gas Cooling and 8.6 Inch Diameter Quartz Chamber

Item Number: TU-DZ13

Maximum Operating Temperature: 1200°C (Inert) / 1000°C (Vacuum) Effective Heating Area: 8.5" ID x 8.5" H (8.6 Liters) Vacuum Capability: 10-4 Torr (Rotary) / 10-5 Torr (Optional Turbo)
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Product Overview

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This high-performance bottom-loading thermal processing system represents a pinnacle of engineering for laboratories and industrial R&D facilities specializing in material science. By utilizing a vertical orientation with a motor-driven sample stage, the equipment provides unparalleled ease of access for loading delicate or heavy samples. The core value of this unit lies in its ability to maintain high vacuum integrity or controlled atmospheric conditions while offering rapid temperature transitions, essential for advanced metallurgical and ceramic research where phase transformations must be tightly controlled.

Designed for versatility, the system is primarily utilized in aerospace, semiconductor, and advanced manufacturing sectors for processes such as vacuum brazing, annealing, and high-temperature synthesis. The equipment is engineered to handle rigorous duty cycles, providing researchers with the confidence that results will remain consistent and reproducible over thousands of hours of operation. Its robust construction combines high-purity quartz technology with precision mechanical lifting components to deliver a reliable thermal environment for the most demanding technical requirements.

Built with safety and efficiency in mind, the unit features an air-cooled double-layer steel casing that ensures the exterior remains safe to touch even during maximum temperature cycles. The integration of high-purity alumina fiber insulation and a high-torque motor for the sample elevator ensures that every cycle is smooth, precise, and thermally efficient. Whether performing basic heat treatment or complex multi-stage vacuum sintering, this system provides the precision and reliability required by modern industrial standards.

Key Features

  • Motor-Driven Bottom Loading Stage: The automated elevator system allows for the seamless insertion and removal of samples, minimizing the risk of thermal shock and physical damage to delicate substrates while ensuring repeatable positioning within the thermal center.
  • Rapid Gas Quenching System: Equipped with a built-in inert gas blow system and four specialized gas delivery tubes, this unit can rapidly cool samples directly after heating, enabling precise control over microstructure development and material hardness.
  • Dual-Zone Temperature Monitoring: Features two independent 30-segment programmable PID controllers; one manages the heating elements while the second monitors the actual sample stage temperature, providing comprehensive data for thermal profile analysis.
  • Electric Radiation Shielding: A motorized sliding door effectively blocks thermal radiation from the heating chamber once the sample stage is lowered, protecting the operator and surrounding equipment while maintaining the internal heat of the chamber.
  • Advanced Vacuum Management: The system integrates a water-cooled SS304 vacuum flange with high-quality O-ring seals, a Pirani gauge for high-sensitivity pressure monitoring, and a dual-stage rotary vane pump to achieve rapid and stable vacuum levels.
  • High-Purity Quartz Chamber: The replaceable 8.5-inch internal diameter quartz chamber provides a clean, non-reactive environment for high-purity processing, capable of operating under both high vacuum and controlled gas flow conditions.
  • Comprehensive Thermal Safety: Engineered with a double-layer steel casing and integrated air cooling, the furnace maintains an exterior surface temperature below 60°C, enhancing lab safety and reducing the load on facility HVAC systems.
  • Precision PID Control Logic: The internal controllers offer auto-tune capabilities, overheating protection, and thermocouple break detection, ensuring that thermal cycles remain within ±1°C of the setpoint for superior process consistency.

Applications

Application Description Key Benefit
Vacuum Brazing Joining of high-performance alloy components or dissimilar metals in a contaminant-free environment. Prevents oxidation and ensures high-strength, clean joints without flux.
Advanced Ceramics Sintering High-temperature densification of technical ceramics under controlled atmosphere or vacuum. Achieves high density and uniform grain structure through precise ramp control.
Thin Film Annealing Post-deposition heat treatment of semiconductor or optical substrates to improve crystalline structure. Minimizes contamination while providing the rapid cooling needed for specific phases.
Metallurgical Research Testing of new alloy compositions and heat treatment cycles including rapid quenching. Allows for precise recreation of industrial quenching processes on a laboratory scale.
Dental Prosthetics Sintering and glazing of dental zirconia and high-strength restorative materials. Exceptional thermal uniformity ensures consistent color and mechanical properties.
Industrial R&D General material synthesis and small-batch production of high-purity powders or components. Flexible atmosphere control permits use with argon, nitrogen, and other inert gases.

Technical Specifications

Parameter Specification Details for TU-DZ13
Model Number TU-DZ13
Power Supply 208 - 240 VAC, Single Phase, 50/60 Hz
Maximum Power Consumption 3600 W (Requires 20 A receptacle)
Max Operating Temperature 1200°C (Inert Gas) / 1000°C (Continuous Vacuum)
Maximum Heating Rate 20°C / minute
Temperature Accuracy ± 1°C
Heating Elements Fe-Cr-Al doped Mo heating elements
Thermocouple Type Dual K-Type thermocouples
Temperature Controllers Two 30-segment programmable PID controllers with RS485 port
Quartz Chamber Dimensions 9" O.D. x 8.5" I.D. x 13.4" H (230 x 218 x 340 mm)
Effective Heating Zone 8.5" I.D. x 8.5" Depth (218 x 216 mm; 8.6 Liters)
Vacuum System Dual-stage rotary vane pump with KF25 port and angle valve
Vacuum Measurement Pirani gauge (10-4 torr) and mechanical vacuum gauge
Cooling System Built-in gas blow quenching system + 16L/min water chiller
Atmosphere Control 5L/min flowmeter with 1/4" gas inlet/outlet
Safety Compliance CE Certified (NRTL / CSA available upon request)
Casing Construction Double-layer steel with air cooling fan
Lifting Mechanism Motor-driven platform with electric sliding radiation door

Why Choose Us

Investing in this bottom-loading vacuum system ensures that your laboratory is equipped with a tool designed for the rigors of modern material science. The unique combination of a large-diameter quartz chamber and a motor-driven elevator allows for the processing of bulky or complex geometries that standard tube furnaces cannot accommodate. By integrating both a high-capacity vacuum pump and an active gas quenching system, the unit provides a level of process control that is typically only found in much larger industrial scale furnaces.

The inclusion of a dedicated water chiller and dual temperature controllers—one specifically for sample monitoring—demonstrates a commitment to engineering excellence that prioritizes data accuracy and equipment longevity. This system is not merely a furnace but a complete thermal processing workstation, built to provide years of consistent service in high-stakes R&D environments. Our technical team is ready to assist with customization to meet your specific atmospheric or vacuum requirements.

Contact us today to receive a technical consultation and a formal quote for your specialized laboratory needs.

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