High Temperature Vertical Atmosphere Controlled Furnace with Automatic Bottom Loading and 1700°C Capacity for Advanced Material Research

Atmosphere Furnace

High Temperature Vertical Atmosphere Controlled Furnace with Automatic Bottom Loading and 1700°C Capacity for Advanced Material Research

Item Number: TU-DZ21

Maximum Temperature: 1700°C Chamber Capacity: 18 Liters (280mm x 300mm) Vacuum Level: 10⁻² Torr
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Product Overview

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This high-performance vertical atmosphere-controlled system represents the pinnacle of precision thermal processing, engineered to meet the rigorous demands of modern material science. Designed with a unique automatic bottom-loading mechanism, the equipment provides a seamless interface for high-temperature sintering, annealing, and melting operations. The unit excels in maintaining atmospheric integrity, allowing researchers to operate under vacuum or specific gas environments with absolute confidence in repeatability and thermal uniformity. By combining a vertical orientation with advanced motorized lifting, the system ensures that samples are handled with the utmost care, minimizing vibration and thermal shock during the loading and unloading phases.

The primary value proposition of this system lies in its ability to reach extreme temperatures of 1700°C while maintaining a safe, water-cooled external environment. It is ideally suited for semiconductor wafer processing, technical ceramic development, and powder metallurgy where atmosphere control is not just a preference but a technical necessity. Target industries include aerospace engineering, semiconductor fabrication, and high-purity chemical processing. The robust construction and integrated cooling technologies ensure that this unit can operate continuously at 1600°C, providing a reliable backbone for any industrial R&D laboratory or small-scale production facility.

Built for long-term operational consistency, the equipment utilizes high-purity fibrous alumina insulation and high-grade Molybdenum Disilicide (MoSi2) heating elements. This combination allows for rapid thermal response and exceptional energy efficiency. Users can rely on the integrated safety protocols, including automatic pressure protection and real-time monitoring, to maintain a secure working environment even during complex, multi-step thermal cycles. This system is more than just a furnace; it is a comprehensive thermal processing solution designed to push the boundaries of material innovation.

Key Features

  • Motorized Bottom-Loading Mechanism: The unit features a precision-engineered electric motor drive that facilitates the automatic lifting and lowering of the bottom flange. This design allows for effortless loading of heavy samples (up to 50 kg) and ensures perfectly centered placement within the thermal zone every time.
  • Advanced MoSi2 Heating Technology: High-grade Molybdenum Disilicide heating elements are strategically positioned to provide superior thermal uniformity. These elements are specifically chosen for their ability to withstand oxidative environments and maintain structural integrity at temperatures up to 1700°C.
  • Dual-Layer Water-Cooled Chamber: The furnace is constructed with a double-layer steel casing that incorporates a water-cooling jacket. This engineering choice protects the vacuum-sealed O-rings and keeps the external skin temperature safe for operators, even during prolonged high-heat cycles.
  • Precision Atmosphere Control: Equipped with a high-quality mechanical vacuum pump and dual flowmeters, the system enables precise control over the internal environment. Users can achieve a vacuum level of 10⁻² torr or maintain a constant positive pressure of inert gases between 100 and 115 KPa.
  • Eurotherm PID Temperature Management: At the heart of the control system is a world-class Eurotherm controller, offering 24 programmable segments. This allows for complex ramping, soaking, and cooling profiles with an accuracy of +/- 0.1°C, ensuring high-yield results for sensitive materials.
  • High-Purity Alumina Insulation: The internal chamber is lined with high-purity fibrous alumina insulation. This low-thermal-mass material ensures maximum energy saving, faster heating rates (up to 10°C/min), and prevents contamination of high-purity samples during the sintering process.
  • Integrated Safety and Protection Systems: The equipment includes built-in PID automatic control with auto-tune functions, overheating protection, and broken thermocouple detection. An automatic pressure release valve is also standard, preventing over-pressurization during gas-assisted processes.
  • Real-Time Data Acquisition: Featuring a built-in RS485 communication port, the system can be fully integrated with a PC for remote monitoring, data logging, and complex program management, providing a digital audit trail for critical research processes.

Applications

Application Description Key Benefit
Semiconductor Wafer Annealing Processing silicon or compound semiconductor wafers under controlled vacuum or inert gas to repair lattice damage. Enhanced electrical properties and structural consistency across the wafer surface.
Technical Ceramic Sintering High-temperature densification of alumina, zirconia, or silicon carbide components in a vertical configuration. Reduced deformation and superior grain size control due to vertical thermal symmetry.
Powder Metallurgy Consolidation of metal powders into solid components under vacuum to prevent oxidation and impurities. High-density parts with excellent mechanical strength and pure chemical composition.
Aerospace Material Testing Subjecting advanced alloys and composites to extreme thermal stress environments to simulate flight conditions. Reliable performance data for flight-critical components under extreme 1700°C environments.
Glass Melting & Research Small-scale melting of specialty glass formulations in high-purity crucibles with precise cooling control. Minimal contamination from the heating environment and precise refractive index management.
Brazing & Joining Joining of dissimilar materials using high-temperature filler metals in an oxygen-free atmosphere. Strong, oxidation-free joints with high structural integrity and clean aesthetic finish.

Technical Specifications

Parameter Group Specification Detail Value / Requirement (Model: TU-DZ21)
Temperature Ratings Maximum Operating Temperature 1700°C (< 1 hour)
Continuous Operating Temperature 800°C - 1600°C
Temperature Accuracy +/- 0.1 ºC
Temperature Uniformity +/- 0.5°C
Recommended Heating Rate ≤ 10°C/min
Chamber Construction Heating Chamber Dimensions 280 mm Diameter x 300 mm Height
Effective Volume 18 Liters
Chamber Material Water-cooled SS with fibrous alumina insulation
Loading Mechanism Electric motor-driven bottom loading
Max Load Capacity 50 Kg
Atmosphere & Vacuum Vacuum Level 10⁻² Torr (via included mechanical pump)
Pressure Control Range 100 - 115 KPa (Constant pressure control)
Gas Flow Management Two integrated flowmeters on front panel
Safety Feature Built-in automatic pressure release valve
Control Systems Temperature Controller Eurotherm (PID, 1 program, 24 segments)
Interface Touch screen control panel
Thermal Couple B-type
Computer Connectivity RS485 Port (PC control ready)
Power & Utilities Voltage Requirements Single-phase 220 VAC, 50/60Hz
Maximum Power Consumption 13 KW (20 A breaker required)
Water Cooling 16L/min recirculating water chiller (Included)
Compliance Standards CE Certified (NRTL/CSA available)

Why Choose This High Temperature Vertical Furnace

  • Unmatched Thermal Precision: The combination of Eurotherm control logic and MoSi2 heating elements ensures that your materials are processed with the highest degree of accuracy, critical for repeatable R&D results.
  • Industrial-Grade Reliability: Engineered for 24/7 operation in demanding environments, the water-cooled stainless steel vacuum chamber maintains structural integrity and vacuum performance over years of heavy use.
  • Superior Sample Access: The motorized bottom-loading design is not just a convenience; it is a safety and quality feature that allows for precise sample positioning and reduces the risk of thermal shock to the heating elements.
  • Complete Ready-to-Use Solution: Unlike systems that require separate procurement of peripherals, this unit includes the vacuum pump and a high-capacity recirculating water chiller, ensuring immediate deployment upon arrival.
  • Scalable and Customisable: With built-in PC control capabilities and a robust 50kg load capacity, this system bridges the gap between laboratory-scale experimentation and pilot-scale production.

Our engineering team is ready to help you optimize your thermal processes. Contact us today to receive a detailed quote or to discuss how this vertical atmosphere furnace can be customized to meet your specific research requirements.

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