Seven Zone 1200C Split Tube Furnace with Precision Temperature Controller and Quick Flange Vacuum System

Tube Furnace

Seven Zone 1200C Split Tube Furnace with Precision Temperature Controller and Quick Flange Vacuum System

Item Number: TU-50

Maximum Temperature: 1200°C Heating Zones: 7 Independent Zones (35" Constant Temperature Zone) Tube Diameter: 130mm OD (5") Quartz Tube
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Product Overview

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This high-performance thermal processing system is engineered for advanced material science and industrial R&D applications that require precise control over temperature profiles and gradients. By utilizing a unique seven-zone heating architecture, the equipment allows researchers to establish either an exceptionally long constant temperature zone or a highly specific stepped thermal gradient. This versatility makes the unit an essential tool for complex processes such as chemical vapor deposition (CVD), crystal growth, and sophisticated annealing cycles where standard single-zone furnaces fail to provide the necessary spatial temperature resolution.

Designed with the rigors of modern laboratory environments in mind, this system integrates a large-diameter quartz process tube with a split-furnace design for easy sample loading and tube maintenance. The separation of the heating chamber from the electronic control unit ensures long-term component reliability and simplifies the integration into existing laboratory workflows or glovebox environments. Target industries include semiconductor manufacturing, battery technology development, and high-performance ceramics research, where consistency and repeatability are non-negotiable.

Built for demanding 24/7 industrial and academic cycles, this unit provides unparalleled thermal stability and operator safety. The robust structural engineering, combined with advanced high-purity fibrous alumina insulation, ensures that energy efficiency is maximized while external surface temperatures remain safe for personnel. Users can rely on this equipment for critical path experiments where the integrity of the thermal environment directly correlates to the quality of the resulting material data.

Key Features

  • Seven Independent Heating Zones: The equipment features seven distinct 150 mm zones that can be programmed independently. This allows for the creation of a massive 35-inch constant temperature zone or a precise thermal gradient across the 42-inch total heating length, offering unmatched flexibility for vapor transport and localized heating experiments.
  • Large Diameter Processing Chamber: Standardized with a 5-inch (130mm) OD quartz tube, the unit is engineered to accommodate substantial batch sizes or large-scale component heat treatments. The versatile design also supports various tube sizes from 1 inch to 4 inches, allowing the laboratory to adapt the system to specific project requirements.
  • Pneumatic Lift Support Mechanism: To ensure ease of use and prevent operator fatigue, the split-cover is supported by heavy-duty compressed air springs. This allows for smooth, controlled opening and closing during tube replacement or specimen loading, protecting the delicate quartz components from accidental impact.
  • Advanced Touch Screen PID Control: The system is managed via a centralized touch-screen interface that regulates all seven zones simultaneously. Users can save up to 10 unique heat treatment programs, each containing 30 segments, ensuring absolute repeatability between different experiment batches.
  • High-Grade Thermal Metallurgy: Utilizing 1300ºC grade Fe-Cr-Al Alloy elements doped with Molybdenum, the furnace provides rapid heating rates and superior longevity compared to standard heating wires. These high-grade elements are specifically chosen for their resistance to oxidation and thermal fatigue at high operating temperatures.
  • Efficiency-Focused Insulation: The interior is lined with energy-saving high-purity fibrous alumina. This high-performance refractory material minimizes heat loss and allows the furnace to maintain a cold outer shell through its double-layered steel case with integrated air-cooling technology.
  • Simplified Vacuum Sealing: Equipped with stainless steel quick-assembling flanges and an anti-corrosive digital vacuum gauge, the system allows for rapid vacuum setup and breakdown. The inclusion of needle valves and a K25 port ensures the system is ready for immediate integration with vacuum pumps and gas delivery manifolds.
  • Durable Safety Protocols: Built-in protection for overheating and broken thermocouples ensures the system automatically shuts down in the event of a technical failure, safeguarding both the equipment and the valuable samples inside the chamber.

Applications

Application Description Key Benefit
Chemical Vapor Deposition (CVD) Growth of carbon nanotubes, graphene, and thin films using gas precursors at high temperatures. Large tube diameter and multi-zone control ensure uniform film deposition over large substrates.
Physical Vapor Transport (PVT) Moving material from a hot source to a cooler substrate via a controlled thermal gradient. Seven independent zones allow for the fine-tuning of the temperature slope required for crystal growth.
Materials Annealing Thermal stress relief and grain size control in specialty alloys and semiconductor wafers. Split-tube design allows for rapid cooling cycles and easy sample retrieval within vacuum or gas environments.
Sintering of Technical Ceramics High-temperature consolidation of ceramic powders into dense, functional laboratory components. High thermal uniformity prevents cracking and ensures consistent density across large samples.
Battery Electrode Development Calcination and synthesis of anode/cathode materials under controlled atmospheric conditions. Excellent atmosphere control and precision PID tuning ensure chemistry remains stable during processing.
Solid-State Synthesis Synthesis of complex oxides and intermetallic compounds via prolonged high-temperature exposure. Reliable continuous operation at 1100°C allows for multi-day processing cycles without performance drift.

Technical Specifications

Specification Category Parameter Details (TU-50)
Model Identification TU-50 Seven-Zone Split Tube Furnace
Max. Operating Temperature 1200 °C (Short term < 1 hour)
Continuous Working Temp. 1100 °C (Flowing Gas) / 1000 °C (Vacuum < 1 torr)
Max. Heating Rate ≤ 10 °C / min
Heating Zone Configuration 7 independent zones; 150 mm (6") each; Total length 1050 mm (42")
Isothermal Zone Length Max 35" (875 mm) constant temperature zone (within +/- 2 °C)
Process Tube Dimensions Quartz Tube: 130mm OD x 122mm ID x 2000mm L (5" x 79")
Compatible Tube Range Accepts processing tubes from 1" to 5" diameter
Heating Element Material 1300ºC grade Fe-Cr-Al Alloy doped by Mo
Power Requirements AC 208-240V Single Phase, 50/60 Hz; 8.5 KW Max (50A breaker)
Temperature Controller Touch screen digital unit; 7-channel PID control; 10 programs / 30 segments
Accuracy & Precision +/- 1 ºC accuracy; Seven K-type thermocouples (one per zone)
Vacuum System Components SS flanges with quick clamp; Needle valve; K25 port; Digital vacuum gauge
Cooling & Shell Design Double-layer steel case with air cooling (Surface temperature < 60 °C)
Compliance & Safety CE Certified; Integrated over-temp and broken-sensor protection
Communications Built-in RS485 port with included data recording software

Why Choose This Seven-Zone Furnace

  • Industrial-Grade Precision: The seven-zone architecture provides the highest degree of spatial thermal control available in a split tube furnace, making it the preferred choice for researchers who cannot compromise on temperature uniformity.
  • Operational Efficiency: The combination of quick flanges, air-spring-assisted lifting, and comprehensive touch-screen controls reduces the time required for setup and process monitoring, increasing your laboratory's throughput.
  • Premium Material Construction: From the molybdenum-doped heating elements to the high-purity alumina insulation, every component is selected to withstand the rigors of high-temperature service and minimize the total cost of ownership.
  • Flexible Integration: Whether you are performing vacuum processing, atmosphere-controlled synthesis, or multi-channel CVD, this system facilitates easy expansion through its standardized flange ports and optional gas delivery compatibility.
  • Proven Stability and Reliability: Backed by CE certification and a design focused on thermal isolation, this equipment maintains high performance over thousands of hours of operation, ensuring that your research data is consistent year after year.

Contact us today for a technical consultation or a customized quote tailored to your specific material processing requirements.

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