Tube Furnace
Four Zone 1200C Multi Zone Split Tube Furnace with Independent Digital Temperature Controllers for One or Two Inch Processing Tubes
Item Number: TU-44
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Product Overview


This precision-engineered multi-zone heating system provides sophisticated thermal processing capabilities for advanced material science and industrial research and development. Designed as a four-zone split tube furnace, the equipment allows for the creation of precise step thermal gradients or exceptionally long uniform temperature zones by independently adjusting the thermal output of four distinct 100mm segments. The separate temperature control console ensures that electronic components are shielded from radiant heat, enhancing the long-term reliability and operational stability of the entire system during high-temperature cycles up to 1200°C.
Ideal for Vapor Phase Transport (VPT), Chemical Vapor Deposition (CVD), and Physical Vapor Transport (PVT), this unit offers researchers the flexibility to accommodate processing tubes with outside diameters of one or two inches. Its split-hinge design facilitates easy sample loading/unloading and enables rapid cooling, which is essential for certain metallurgical and thin-film growth processes. By integrating high-purity alumina fiber insulation and advanced heating elements, the system achieves remarkable energy efficiency while maintaining a cool exterior surface temperature for operator safety.
Built for demanding laboratory environments, the equipment emphasizes consistency and reproducibility. Each of the four zones is governed by its own dedicated digital controller, allowing for complex temperature profiles that are essential for growing high-quality crystals and synthesizing novel materials. Whether used in a horizontal configuration for standard processing or mounted vertically for specialized applications, the unit delivers the robustness and precision required for critical industrial research and high-stakes material characterization.
Key Features
- Independently Controlled Four-Zone Heating: The system features four separate 100mm heating zones, each equipped with its own dedicated PID controller. This architecture allows users to establish specific temperature gradients or extend the constant temperature zone to up to 250mm with ±1°C accuracy.
- Advanced Thermal Insulation and Shell Design: A double-layered steel case integrated with air-cooling technology maintains the exterior surface temperature below 60°C. The internal chamber utilizes energy-saving, high-purity fibrous alumina insulation that minimizes heat loss and improves temperature response times.
- High-Performance Alloy Heating Elements: Equipped with 1300°C grade Fe-Cr-Al alloy elements doped with Molybdenum, the furnace ensures long-lasting operation and can reach peak temperatures of 1200°C with rapid heating rates of up to 20°C per minute.
- Precision PID Digital Controllers: The control console includes four individual digital units featuring PID automatic control for heating, cooling, and dwell times. Each controller supports up to 30 programmable segments, providing granular control over complex thermal sequences.
- Split Furnace Architecture: The split-hinge design allows for the rapid opening of the furnace, which is critical for experimental setups requiring quick access to the processing tube or for accelerating cooling rates to quench materials after high-temperature treatment.
- Versatile Mounting Configurations: The heating module is engineered for flexibility, capable of being positioned horizontally or vertically depending on the specific experimental requirements, such as vertical Bridgman crystal growth or horizontal CVD processes.
- Integrated Safety and Monitoring: Built-in protection against overheating and broken thermocouples ensures the system shuts down safely in the event of a fault, protecting both the equipment and the sensitive samples within the processing tube.
- Scalable Communication Interfaces: Standard RS485 communication ports allow for potential integration with external PC software for remote monitoring, data logging, and complex program synchronization across all heating zones.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| CVD / PECVD | Chemical Vapor Deposition of thin films and nanomaterials where precise precursor evaporation and deposition temperatures are required. | Precise thermal gradients ensure optimal reaction kinetics and film uniformity. |
| Physical Vapor Transport | Harvesting synthetic crystals by vaporizing a source material at high temp and depositing it at a cooler zone. | Four independent zones allow for the exact temperature difference needed for high-purity crystal growth. |
| Annealing Treatment | Controlled heat treatment of metallic and ceramic samples to relieve internal stresses and modify mechanical properties. | Split design enables controlled cooling rates to achieve specific material microstructures. |
| Semiconductor Doping | High-temperature diffusion of dopants into semiconductor wafers or substrates using gaseous precursors. | Consistent uniform temperature zone lengths up to 250mm ensure batch homogeneity. |
| Calcination & Sintering | Thermal processing of catalyst materials or ceramic powders at temperatures up to 1100°C. | Digital control ensures repeatable thermal cycles for consistent material batch quality. |
| Vacuum Heat Treatment | Processing sensitive materials under high vacuum or inert atmospheres to prevent oxidation. | Specialized vacuum flanges and thermal blocks support secure operation down to 10-5 torr. |
| Crystal Growth (Bridgman) | Employing vertical orientation to slowly move materials through a temperature gradient for single crystal formation. | Modular heating zones provide the necessary gradient stability for consistent grain boundary control. |
Technical Specifications
| Parameter | Specification for TU-44 |
|---|---|
| Model Number | TU-44 |
| Furnace Structure | Double layer steel case with air cooling; High purity fibrous alumina insulation |
| Max. Working Temperature | 1200ºC (< 1 Hour, without vacuum) |
| Continuous Temperature | 1100ºC |
| Max. Heating Rate | ≤ 20ºC / min |
| Heating Element | 1300ºC grade Fe-Cr-Al Alloy doped by Mo |
| Total Heating Chamber Length | 400 mm |
| Heating Zone Configuration | Four (4) independent zones, 100 mm each |
| Constant Temp Zone Length | Max 250 mm (± 1°C) if all 4 zones are at same temp |
| Max. Zone Temperature Diff. | 200°C between adjacent zones |
| Temperature Accuracy | ± 1 ºC |
| Temperature Controllers | 4 sets of Digital PID controllers; 30 programmable segments |
| Thermocouple Type | Four K-type thermocouples (one per zone) |
| Voltage & Power | AC 110V Single Phase, 50/60 Hz, 30 A (3 KW Max) |
| External Electrical Note | Use 5000W transformer for 208-240V; Never use NEMA 5-15/20R wall outlet |
| Processing Tube Diameter | Accommodates 1” or 2” OD tubes (min. 1000mm length) |
| Max. Vacuum Level | ≤ 1000°C for vacuum use; < 0.2 bar for low pressure gas |
| Certifications | CE Certified (NRTL or CSA available upon request) |
| Communication | RS485 port standard (Remote Software optional) |
Why Choose Us
- Superior Thermal Flexibility: The four-zone architecture provides a level of gradient control that is impossible with single-zone systems, making it the preferred choice for complex vapor phase synthesis and high-purity crystal growth.
- Separable Control Architecture: By isolating the control electronics into a separate console, we prevent thermal drifting of the electronics and extend the life of the PID controllers, ensuring consistent performance over years of industrial use.
- Precision Engineering and Build Quality: From the Mo-doped heating elements to the air-cooled double-shell casing, every component of this unit is selected for durability in demanding research and production environments.
- Modular and Customizable: The system can be easily adapted with optional vacuum flanges, digital gauges, and various tube materials, and is compatible with both horizontal and vertical experimental setups.
- Safety and Compliance: With full CE certification and built-in protection mechanisms for thermocouples and over-temperature events, this equipment meets the rigorous safety standards required by modern laboratories and manufacturing facilities.
Looking for a specialized thermal profile or custom configuration for your research? Contact our engineering team today for a technical consultation or a formal quotation tailored to your specifications.
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