Tube Furnace
1500C Eight Zone Split Tube Furnace for Thermal Gradient Processing and Advanced Material Research
Item Number: TU-68
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Product Overview

This high-temperature thermal processing system is engineered specifically for sophisticated material science applications where precise temperature gradients and high-throughput research are paramount. By integrating eight independently controlled heating zones, the equipment allows for the creation of complex thermal profiles that are impossible to achieve with single-zone or even three-zone furnaces. This capability is essential for the development of gradient functional materials and the study of multi-phase transition re-crystallization, providing researchers with the flexibility to simulate real-world industrial cooling and heating cycles in a controlled laboratory environment.
Designed for reliability in demanding industrial R&D settings, the system utilizes a high-purity mullite ceramic tube and a split-chamber configuration. This design facilitates easy access to the reaction zone, enabling rapid sample loading and the integration of complex experimental setups. The unit’s robust silicon carbide heating elements ensure consistent performance up to 1500°C, while the secondary safety layers, including over-temperature protection and automatic alarms, allow for extended operation without continuous supervision. This makes the system an indispensable tool for advanced ceramics, metallurgy, and semiconductor research.
Operating with extreme stability, the equipment maintains a high-purity atmosphere or vacuum environment, supporting research into catalytic graphitization and the evolution of pore structures in carbon-based materials. Every component, from the touch-screen temperature controllers to the precision-machined flanges, is selected to meet the rigorous standards of premium laboratory engineering. This unit offers a versatile platform for researchers who demand precision, repeatability, and the ability to scale their thermal processes from early-stage discovery to reproducible industrial prototypes.
Key Features
- Eight-Channel Independent Zone Control: Each of the eight heating zones is managed by a dedicated touch-screen PID controller, allowing for the creation of steep or gentle thermal gradients up to 1500°C with unmatched spatial precision.
- Advanced Thermal Gradient Tuning: The system can achieve a maximum temperature gradient of 100°C per inch, a capability further enhanced by the ability to insert thermal insulation spacing elements between zones for customized heat field profiling.
- High-Performance Silicon Carbide Elements: Equipped with 16 1500°C-grade SiC rods, the chamber delivers rapid heating rates and provides the thermal density necessary to maintain stable temperatures across the entire 400mm heating length.
- Precision Mullite Ceramic Reaction Tube: The unit includes a high-purity USA-made mullite tube (84mm O.D.), specifically selected for its thermal shock resistance and chemical stability under vacuum and low-pressure conditions.
- Modern Human-Machine Interface: The integrated touch-screen controllers feature 30 programmable segments for precise automation of heating rates, cooling rates, and dwell times, complete with data logging features via RS485 communication.
- Split-Chamber Engineering Excellence: The furnace housing features a split-opening design that allows the user to open the heating chamber lengthwise, facilitating the installation of pre-assembled tubes, thermocouples, and sensors without disturbing delicate samples.
- Vacuum and Atmosphere Versatility: Optimized for low-pressure environments, the equipment maintains a vacuum level of 10E-2 torr with mechanical pumps and can reach 10-5 torr with molecular systems, supported by high-quality vacuum flanges and seals.
- Redundant Safety Systems: Built-in over-temperature protection, thermocouple failure alarms, and emergency shut-off protocols ensure the safety of both the laboratory personnel and the high-value materials being processed.
- Scalable Digital Monitoring: Optional Labview-based software and WiFi control enable remote monitoring and management of heat-treatment recipes across a 300-meter range, ideal for modern networked research facilities.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Gradient Functional Materials | Synthesis of materials with spatially varying properties by applying different temperatures across the sample length. | Precise control over mechanical and chemical gradients within a single processing run. |
| Phase Transition Studies | Investigation of high-throughput phase changes and re-crystallization kinetics across multiple temperature points simultaneously. | Accelerated research timelines by collecting data from multiple temperature zones in one cycle. |
| Catalytic Graphitization | High-temperature processing of carbon and catalyst mixtures to transform amorphous carbon into graphite structures. | Superior thermal field uniformity ensures even transformation and consistent pore structure development. |
| Semiconductor CVD Support | Providing a stable thermal environment for chemical vapor deposition processes requiring large-area temperature uniformity. | High-accuracy PID control prevents local overheating and ensures deposition consistency. |
| Ceramic Co-firing | Sintering of complex ceramic components that require specific zones of heating to manage differential shrinkage. | Independent zone control reduces internal stress and prevents cracking in ceramic-metal composites. |
| Aerospace Alloy Research | Testing heat-resistant alloys under high-temperature gradients to simulate jet engine environments. | Reliable 1500°C capability allows for testing under realistic extreme operational conditions. |
| Nuclear Material Testing | Simulating thermal profiles found in reactor cores for the testing of cladding and structural materials. | Robust SiC elements and mullite tubes offer the durability required for long-duration heavy thermal cycling. |
Technical Specifications
| Parameter | Specification Details for Model TU-68 |
|---|---|
| Product Model Identifier | TU-68 |
| Power Rating | 9.0 kW |
| Operating Voltage | AC 208 - 240V, Single Phase, 50/60Hz (Requires 50A Breaker) |
| Maximum Working Temperature | 1500°C |
| Continuous Working Temperature | 1400°C |
| Recommended Heating Rate | ≤ 5°C / min |
| Processing Tube Material | High-Purity Mullite Ceramic (Made in USA) |
| Processing Tube Dimensions | 84mm O.D. x 73mm I.D. x 1219mm Length |
| Heating Zone Configuration | Eight Zones (50mm per zone, including 20mm spacing) |
| Total Heating Zone Length | 400 mm |
| Constant Temperature Zone | 300 mm (When all zones are set to identical temperature) |
| Temperature Accuracy | +/- 1ºC |
| Max Thermal Gradient | 100°C / inch |
| Temperature Controller | 8-Channel Touch Screen PID; 30 Programmable Segments |
| Sensors | 8 x S-type Thermocouples (One per heating zone) |
| Heating Elements | 16 x 1500ºC Grade Silicon Carbide (SiC) Rods |
| Vacuum Levels | 10E-2 Torr (Mechanical Pump) / 10-5 Torr (Molecular Pump) |
| Maximum Gas Pressure | < 0.02 Mpa (Low pressure environment only) |
| Communication Interface | RS485 Port for Laptop/Data System connectivity |
| Compliance | CE Certified (NRTL or CSA available upon request) |
Why Choose TU-68
- Unmatched Spatial Control: The eight-zone architecture provides the highest degree of spatial thermal control in the industry, allowing for gradients and high-throughput research that standard furnaces cannot match.
- Premium Material Integration: By utilizing USA-made mullite tubes and 1500°C-grade SiC elements, this system is built to survive years of continuous, high-temperature cycling without degradation.
- Precision-Engineered Consistency: With a temperature accuracy of +/- 1ºC and independent PID loops for every zone, researchers can trust that their data is accurate and every process is repeatable.
- Highly Versatile and Adaptable: Whether your research requires a high vacuum, an inert gas atmosphere, or specific thermal gradient tuning via insulation spacers, this system adapts to your experimental needs.
- Support and Customization: THERMUNITS provides comprehensive technical support to help you configure thermal profiles and offers optional software integrations for advanced automation and remote monitoring.
To discuss your specific thermal processing requirements or to request a detailed quote for this advanced system, please contact our technical sales team today.
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